9H-Thioxanthen-3-ol, 7-chloro-9-(3-(dimethylamino)propylidene)-, (Z)-

Base Information

Chemical Name:9H-Thioxanthen-3-ol, 7-chloro-9-(3-(dimethylamino)propylidene)-, (Z)-
CAS No.:77602-73-4
Molecular Formula:C₁₈H₁₈ClNOS
Molecular Weight:331.866
Hs Code.:2932999099
DSSTox Substance ID:DTXSID20228269
Wikidata:Q76388059
Mol file:77602-73-4.mol

Synonyms:77602-73-4;9H-Thioxanthen-3-ol, 7-chloro-9-(3-(dimethylamino)propylidene)-, (Z)-;BRN 4704374;VUFB-12364;(9Z)-7-chloro-9-[3-(dimethylamino)propylidene]thioxanthen-3-ol;(Z)-2-Chloro-6-hydroxy-9-(3-dimethylaminopropylidene)thioxanthene;(Z)-7-Chloro-9-(3-(dimethylamino)propylidene)-9H-thioxanthen-3-ol;DTXSID20228269;WHGUGQZTJWCKGG-CPSFFCFKSA-N;LS-153672;AE-641/00360047;7-chloro-9-[3-(dimethylamino)propylidene]-9H-thioxanthen-3-ol

Suppliers and Price of 9H-Thioxanthen-3-ol, 7-chloro-9-(3-(dimethylamino)propylidene)-, (Z)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(Z)-2-CHLORO-6-HYDROXY-9-(3-DIMETHYLAMINOPROPYLIDENE)THIOXANTHENE 95.00%
5MG
$ 503.28

Total 4 raw suppliers

Chemical Property of 9H-Thioxanthen-3-ol, 7-chloro-9-(3-(dimethylamino)propylidene)-, (Z)-

Chemical Property:

Vapor Pressure:5.45E-10mmHg at 25°C
Boiling Point:484°C at 760 mmHg
Flash Point:246.5°C
PSA：48.77000
Density:1.327g/cm³
LogP:4.89360
XLogP3:4.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:331.0797631
Heavy Atom Count:22
Complexity:414

Purity/Quality:

99% ^*data from raw suppliers

(Z)-2-CHLORO-6-HYDROXY-9-(3-DIMETHYLAMINOPROPYLIDENE)THIOXANTHENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)CCC=C1C2=C(C=C(C=C2)O)SC3=C1C=C(C=C3)Cl
Isomeric SMILES:CN(C)CC/C=C\1/C2=C(C=C(C=C2)O)SC3=C1C=C(C=C3)Cl

Technology Process of 9H-Thioxanthen-3-ol, 7-chloro-9-(3-(dimethylamino)propylidene)-, (Z)-

There total 4 articles about 9H-Thioxanthen-3-ol, 7-chloro-9-(3-(dimethylamino)propylidene)-, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 77602-62-1
2-chloro-6-methoxy-9-(3-dimethylaminopropylidene)thioxanthene

: 77602-73-4
2-chloro-6-hydroxy-9-(3-dimethylaminopropylidene)thioxanthene

Guidance literature:: With boron tribromide; In dichloromethane; for 6h; Ambient temperature;
DOI:10.1135/cccc19803166

Reference yield: 13.0%

: 77602-56-3
2-chloro-6-methoxy-9-(3-dimethylaminopropyl)thioxanthene-9-ol

: 77602-73-4
2-chloro-6-hydroxy-9-(3-dimethylaminopropylidene)thioxanthene

Guidance literature:: With hydrogen bromide; In acetic acid; for 6h; Heating;
DOI:10.1135/cccc19803166

Reference yield:

: 54506-90-0
2-(4-chlorophenylthio)-4-methoxybenzoic acid

: 77602-73-4
2-chloro-6-hydroxy-9-(3-dimethylaminopropylidene)thioxanthene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / polyphosphoric acid / 3 h / 125 - 135 °C

2: 1) Mg / 1) THF

3: 13 percent / HBr / acetic acid / 6 h / Heating

With PPA; hydrogen bromide; magnesium; In acetic acid;
DOI:10.1135/cccc19803166