trans-2-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1-methyl-1-<4'-methyl-3'-(1'''-methylvinyl)pent-3'-enyl>cyclohexane

Base Information

Chemical Name:trans-2-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1-methyl-1-<4'-methyl-3'-(1'''-methylvinyl)pent-3'-enyl>cyclohexane
CAS No.:115819-60-8
Molecular Formula:C₂₅H₄₆OSi
Molecular Weight:390.725
Hs Code.:

Synonyms:trans-2-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1-methyl-1-<4'-methyl-3'-(1'''-methylvinyl)pent-3'-enyl>cyclohexane

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Chemical Property of trans-2-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1-methyl-1-<4'-methyl-3'-(1'''-methylvinyl)pent-3'-enyl>cyclohexane

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Technology Process of trans-2-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1-methyl-1-<4'-methyl-3'-(1'''-methylvinyl)pent-3'-enyl>cyclohexane

There total 4 articles about trans-2-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1-methyl-1-<4'-methyl-3'-(1'''-methylvinyl)pent-3'-enyl>cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 115842-84-7
trans-5-<2'-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1'-methylcyclohexyl>-3-(1'''-methyl-1'''-phenylselenoethyl)-2-methylpent-1-en-3-ol

: 115819-60-8
trans-2-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1-methyl-1-<4'-methyl-3'-(1'''-methylvinyl)pent-3'-enyl>cyclohexane

Guidance literature:: With thionyl chloride; triethylamine; In dichloromethane; for 2h; Ambient temperature;

Reference yield:

: 109263-23-2,115889-37-7
3-{(1R,2S)-2-[1-(tert-Butyl-dimethyl-silanyloxy)-allyl]-1-methyl-cyclohexyl}-propionaldehyde

: 115819-60-8
trans-2-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1-methyl-1-<4'-methyl-3'-(1'''-methylvinyl)pent-3'-enyl>cyclohexane

Guidance literature:: Multi-step reaction with 4 steps

1: 68 percent / tetrahydrofuran / 0.5 h / Ambient temperature

2: 74 percent / chromium trioxide, pyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 85 percent / butyl-lithium / tetrahydrofuran / -78 deg C, 1 h, room temperature, 1 h

4: 54 percent / thionyl chloride, triethylamine / CH₂Cl₂ / 2 h / Ambient temperature

With pyridine; chromium(VI) oxide; n-butyllithium; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 115819-56-2
trans-5-<2'-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1'-methylcyclohexyl>-2-methylpent-1-en-3-ol

: 115819-60-8
trans-2-<1''-(dimethyl-t-butylsiloxy)prop-2''-enyl>-1-methyl-1-<4'-methyl-3'-(1'''-methylvinyl)pent-3'-enyl>cyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / chromium trioxide, pyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 85 percent / butyl-lithium / tetrahydrofuran / -78 deg C, 1 h, room temperature, 1 h

3: 54 percent / thionyl chloride, triethylamine / CH₂Cl₂ / 2 h / Ambient temperature

With pyridine; chromium(VI) oxide; n-butyllithium; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane;