1-benzyl-4-((4-phenyl-1H-1, 2, 3-triazol-1-yl)methyl)-1H-1, 2, 3-triazole

Base Information

Chemical Name:1-benzyl-4-((4-phenyl-1H-1, 2, 3-triazol-1-yl)methyl)-1H-1, 2, 3-triazole
CAS No.:1338831-33-6
Molecular Formula:C₁₈H₁₆N₆
Molecular Weight:316.365
Hs Code.:

Synonyms:1-benzyl-4-((4-phenyl-1H-1, 2, 3-triazol-1-yl)methyl)-1H-1, 2, 3-triazole

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Chemical Property of 1-benzyl-4-((4-phenyl-1H-1, 2, 3-triazol-1-yl)methyl)-1H-1, 2, 3-triazole

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Technology Process of 1-benzyl-4-((4-phenyl-1H-1, 2, 3-triazol-1-yl)methyl)-1H-1, 2, 3-triazole

There total 4 articles about 1-benzyl-4-((4-phenyl-1H-1, 2, 3-triazol-1-yl)methyl)-1H-1, 2, 3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1338831-18-7
C₁₇H₁₇N₃O₃S

: 536-74-3
phenylacetylene

: 1338831-33-6
1-benzyl-4-((4-phenyl-1H-1, 2, 3-triazol-1-yl)methyl)-1H-1, 2, 3-triazole

Guidance literature:: C₁₇H₁₇N₃O₃S; With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

phenylacetylene; With copper(l) iodide; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.09.004

Reference yield: 57.0%

: 1472651-87-8
4-(azidomethyl)-1-benzyl-1H-1,2,3-triazole

: 536-74-3
phenylacetylene

: 1338831-33-6
1-benzyl-4-((4-phenyl-1H-1, 2, 3-triazol-1-yl)methyl)-1H-1, 2, 3-triazole

Guidance literature:: With ((1-(4-methoxy)benzyl)-1H-1,2,3-triazol-4-yl)methanol; copper(II) sulfate; sodium L-ascorbate; In water; dimethyl sulfoxide; at 20 ℃; for 4h;
DOI:10.1016/j.tetlet.2015.09.010

Reference yield:

: 28798-81-4
(1-benzyl-[1,2,3]triazol-4-yl)methanol

: 1338831-33-6
1-benzyl-4-((4-phenyl-1H-1, 2, 3-triazol-1-yl)methyl)-1H-1, 2, 3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.1: sodium azide / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With sodium azide; potassium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.09.004