5-<<4-phenyl>sulfonyl>pentanoic acid

Base Information

Chemical Name:5-<<4-phenyl>sulfonyl>pentanoic acid
CAS No.:130199-01-8
Molecular Formula:C₁₅H₂₁Cl₂NO₄S
Molecular Weight:382.308
Hs Code.:

5-<<4-<N,N-bis(2-chloroethyl)amino>phenyl>sulfonyl>pentanoic acid

Synonyms:5-<<4-phenyl>sulfonyl>pentanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-<<4-phenyl>sulfonyl>pentanoic acid

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Technology Process of 5-<<4-phenyl>sulfonyl>pentanoic acid

There total 10 articles about 5-<<4-phenyl>sulfonyl>pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 130198-95-7
methyl 5-<<4-phenyl>sulfonyl>pentanoate

: 130199-01-8
5-<<4-phenyl>sulfonyl>pentanoic acid

Guidance literature:: With hydrogenchloride; for 2h; Heating;
DOI:10.1021/jm00173a016

Reference yield:

: 5454-83-1
5-bromovaleric acid methyl ester

: 130199-01-8
5-<<4-phenyl>sulfonyl>pentanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / K₂CO₃ / methanol / 0.17 h / Heating

2: Et₃N / CH₂Cl₂ / 0.75 h / 0 °C

3: NaCl / dimethylformamide / 0.08 h / 120 °C

4: 78 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 20 h / 20 °C

5: 99 percent / concd. HCl / 2 h / Heating

With hydrogenchloride; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium chloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00173a016

Reference yield:

: 100132-31-8
4-benzenethiol

: 130199-01-8
5-<<4-phenyl>sulfonyl>pentanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / K₂CO₃ / methanol / 0.17 h / Heating

2: Et₃N / CH₂Cl₂ / 0.75 h / 0 °C

3: NaCl / dimethylformamide / 0.08 h / 120 °C

4: 78 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 20 h / 20 °C

5: 99 percent / concd. HCl / 2 h / Heating

With hydrogenchloride; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium chloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00173a016