Technology Process of rac-1-amino-2-ethoxy-3-(trityloxy)propane
There total 3 articles about rac-1-amino-2-ethoxy-3-(trityloxy)propane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrazine hydrate;
In
methanol;
for 3h;
Yield given;
Heating;
DOI:10.1021/jm00108a021
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 63.9 percent / pyridine / CH2Cl2 / Ambient temperature
2: 68.4 percent / 4-(dimethylamino)pyridine (DMAP) / CH2Cl2 / Ambient temperature
3: dimethylsulfoxide / 55 °C
4: H2NNH2*H2O / methanol / 3 h / Heating
With
pyridine; dmap; hydrazine hydrate;
In
methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm00108a021
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 68.4 percent / 4-(dimethylamino)pyridine (DMAP) / CH2Cl2 / Ambient temperature
2: dimethylsulfoxide / 55 °C
3: H2NNH2*H2O / methanol / 3 h / Heating
With
dmap; hydrazine hydrate;
In
methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/jm00108a021
