4-[tert-butoxycarbonyl-(4-trifluoromethoxy-benzyl)-amino]-3-nitro-benzoic acid allyl ester

Base Information

• Chemical Name: 4-[tert-butoxycarbonyl-(4-trifluoromethoxy-benzyl)-amino]-3-nitro-benzoic acid allyl ester
• CAS No.: 885232-39-3
• Molecular Formula: C₂₃H₂₃F₃N₂O₇
• Molecular Weight: 496.44

Synonyms:4-[tert-butoxycarbonyl-(4-trifluoromethoxy-benzyl)-amino]-3-nitro-benzoic acid allyl ester

Chemical Property of 4-[tert-butoxycarbonyl-(4-trifluoromethoxy-benzyl)-amino]-3-nitro-benzoic acid allyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 4-[tert-butoxycarbonyl-(4-trifluoromethoxy-benzyl)-amino]-3-nitro-benzoic acid allyl ester

There total 1 articles about 4-[tert-butoxycarbonyl-(4-trifluoromethoxy-benzyl)-amino]-3-nitro-benzoic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-nitro-4-(4-trifluoromethoxy-benzylamino)-benzoic acid allyl ester (885232-38-2) + di-tert-butyl dicarbonate (24424-99-5) → 4-[tert-butoxycarbonyl-(4-trifluoromethoxy-benzyl)-amino]-3-nitro-benzoic acid allyl ester (885232-39-3)

Guidance literature:

With 2-(Dimethylamino)pyridine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield:

4-[tert-butoxycarbonyl-(4-trifluoromethoxy-benzyl)-amino]-3-nitro-benzoic acid allyl ester (885232-39-3) → 3-amino-4-[tert-butoxycarbonyl-(4-trifluoromethoxy-benzyl)-amino]-benzoic acid allyl ester (885232-40-6)

Guidance literature:

With tin(ll) chloride; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

upstream raw materials:

3-nitro-4-(4-trifluoromethoxy-benzylamino)-benzoic acid allyl ester

di-tert-butyl dicarbonate

Downstream raw materials:

3-amino-4-[tert-butoxycarbonyl-(4-trifluoromethoxy-benzyl)-amino]-benzoic acid allyl ester

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