4-[5'-(5,5-dimethyl-1,3-dioxan-2-yl)-2,2'-bithiophen-5-yl]-N,N-bis(9,9-dimethyl-7-nonylfluoren-2-yl)benzeneamine

Base Information

• Chemical Name: 4-[5'-(5,5-dimethyl-1,3-dioxan-2-yl)-2,2'-bithiophen-5-yl]-N,N-bis(9,9-dimethyl-7-nonylfluoren-2-yl)benzeneamine
• CAS No.: 1097177-23-5
• Molecular Formula: C₆₈H₈₁NO₂S₂
• Molecular Weight: 1008.53

Synonyms:4-[5'-(5,5-dimethyl-1,3-dioxan-2-yl)-2,2'-bithiophen-5-yl]-N,N-bis(9,9-dimethyl-7-nonylfluoren-2-yl)benzeneamine

Chemical Property of 4-[5'-(5,5-dimethyl-1,3-dioxan-2-yl)-2,2'-bithiophen-5-yl]-N,N-bis(9,9-dimethyl-7-nonylfluoren-2-yl)benzeneamine

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Technology Process of 4-[5'-(5,5-dimethyl-1,3-dioxan-2-yl)-2,2'-bithiophen-5-yl]-N,N-bis(9,9-dimethyl-7-nonylfluoren-2-yl)benzeneamine

There total 1 articles about 4-[5'-(5,5-dimethyl-1,3-dioxan-2-yl)-2,2'-bithiophen-5-yl]-N,N-bis(9,9-dimethyl-7-nonylfluoren-2-yl)benzeneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

4,4,5,5-tetramethyl-2-(5-(5-(5,5-dimethyl-1,3-dioxan-2-yl)thiophen-2-yl)-thiophen-2-yl)-1,3,2-dioxaborolane (1086450-04-5) + N,N-bis(9,9-dimethyl-7-nonylfluoren-2-yl)-4-bromoaniline (1097177-16-6) → 4-[5'-(5,5-dimethyl-1,3-dioxan-2-yl)-2,2'-bithiophen-5-yl]-N,N-bis(9,9-dimethyl-7-nonylfluoren-2-yl)benzeneamine (1097177-23-5)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; for 12h; Reflux;

DOI:10.1039/b811401c

Reference yield: 94.0%

4-[5'-(5,5-dimethyl-1,3-dioxan-2-yl)-2,2'-bithiophen-5-yl]-N,N-bis(9,9-dimethyl-7-nonylfluoren-2-yl)benzeneamine (1097177-23-5) → C63H71NOS2 (1097177-29-1)

Guidance literature:

With trifluoroacetic acid; In tetrahydrofuran; water; at 20 ℃; for 2h;

DOI:10.1039/b811401c

upstream raw materials:

4,4,5,5-tetramethyl-2-(5-(5-(5,5-dimethyl-1,3-dioxan-2-yl)thiophen-2-yl)-thiophen-2-yl)-1,3,2-dioxaborolane

N,N-bis(9,9-dimethyl-7-nonylfluoren-2-yl)-4-bromoaniline

Downstream raw materials:

C₆₃H₇₁NOS₂

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