1-(3-bromo-4-methoxyphenyl)-2,2-diiodoethanone

Base Information

Chemical Name:1-(3-bromo-4-methoxyphenyl)-2,2-diiodoethanone
CAS No.:1374568-36-1
Molecular Formula:C₉H₇BrI₂O₂
Molecular Weight:480.866
Hs Code.:

Synonyms:1-(3-bromo-4-methoxyphenyl)-2,2-diiodoethanone

Suppliers and Price of 1-(3-bromo-4-methoxyphenyl)-2,2-diiodoethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(3-bromo-4-methoxyphenyl)-2,2-diiodoethanone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(3-bromo-4-methoxyphenyl)-2,2-diiodoethanone

There total 2 articles about 1-(3-bromo-4-methoxyphenyl)-2,2-diiodoethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1374568-21-4
1-(3-bromo-4-methoxyphenyl)-2,2-diiodoethanol

: 1374568-36-1
1-(3-bromo-4-methoxyphenyl)-2,2-diiodoethanone

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 20 ℃; for 19h;
DOI:10.1002/ejoc.201101835

Reference yield:

: 34841-06-0
3-bromo-4-methoxybenzylaldehyde

: 1374568-36-1
1-(3-bromo-4-methoxyphenyl)-2,2-diiodoethanone

Guidance literature:: Multi-step reaction with 2 steps

1: isopropylmagnesium chloride / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 19 h / 20 °C

With isopropylmagnesium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1002/ejoc.201101835

Reference yield:

: 1374568-36-1
1-(3-bromo-4-methoxyphenyl)-2,2-diiodoethanone

: 1196105-19-7
2-(3-bromo-4-methoxyphenyl)quinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyl sulfoxide / 40 h / 60 °C

2: acetic acid / ethanol / 1 h / 90 °C

With acetic acid; dimethyl sulfoxide; In ethanol;
DOI:10.1002/ejoc.201101835