Ethyl 1-methyl-4-oxocyclohexanepropanoate

Base Information

Chemical Name:Ethyl 1-methyl-4-oxocyclohexanepropanoate
CAS No.:60547-67-3
Molecular Formula:C₁₂H₂₀O₃
Molecular Weight:212.289
Hs Code.:
DSSTox Substance ID:DTXSID001271062

Synonyms:60547-67-3;DTXSID001271062;Ethyl 1-methyl-4-oxocyclohexanepropanoate

Suppliers and Price of Ethyl 1-methyl-4-oxocyclohexanepropanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl 1-methyl-4-oxocyclohexanepropanoate

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:212.14124450
Heavy Atom Count:15
Complexity:235

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)CCC1(CCC(=O)CC1)C

Technology Process of Ethyl 1-methyl-4-oxocyclohexanepropanoate

There total 3 articles about Ethyl 1-methyl-4-oxocyclohexanepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 127603-04-7
ethyl-3-(1-methyl-4-oxocyclohex-2-enyl)propionate

: 60547-67-3
ethyl-3-(1-methyl-4-oxocyclohexyl)propionate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0040-4020(01)89151-1

Reference yield:

: 57404-75-8
ethyl 4-formylpentanoate

: 60547-67-3
ethyl-3-(1-methyl-4-oxocyclohexyl)propionate

Guidance literature:: Multi-step reaction with 2 steps

1: 4.) acetic acid / 1.) piperidine/benzene, reflux; 2.) 5 deg C, overnight; 3.) reflux, 16 h; 4.) reflux 6 h

2: 96 percent / hydrogen / 10 percent Pd/C / ethanol

With hydrogen; acetic acid; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0040-4020(01)89151-1

Reference yield:

: 140-88-5,9003-32-1
ethyl acrylate

: 60547-67-3
ethyl-3-(1-methyl-4-oxocyclohexyl)propionate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) K₂CO₃ / 1.) piperidine, r.t., 2 h; 2.) benzene, r.t., 4 h; 3.) reflux, 36 h

2: 4.) acetic acid / 1.) piperidine/benzene, reflux; 2.) 5 deg C, overnight; 3.) reflux, 16 h; 4.) reflux 6 h

3: 96 percent / hydrogen / 10 percent Pd/C / ethanol

With hydrogen; potassium carbonate; acetic acid; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0040-4020(01)89151-1