Technology Process of C30H27NO5S
There total 7 articles about C30H27NO5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 0 ℃;
for 0.5h;
DOI:10.1021/ja00049a022
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 92 percent / cesium carbonate, 18-crown-6 / acetonitrile / 10 h / Ambient temperature
2: 0.5 N aq. LiOH / tetrahydrofuran / 0.5 h / 0 °C
3: triphenylphosphine / CH2Cl2 / 0.5 h / 0 °C
4: 68 percent / sodium borohydride / CH2Cl2; propan-2-ol / 0.5 h / 0 °C
5: 99 percent / 2,6-lutidine / CH2Cl2 / 1 h / -78 - 0 °C
6: 98 percent / NaH / tetrahydrofuran / 0.08 h / 0 °C
7: 96 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C
With
2,6-dimethylpyridine; lithium hydroxide; sodium tetrahydroborate; 18-crown-6 ether; tetrabutyl ammonium fluoride; sodium hydride; caesium carbonate; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; isopropyl alcohol; acetonitrile;
DOI:10.1021/ja00049a022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 99 percent / 2,6-lutidine / CH2Cl2 / 1 h / -78 - 0 °C
2: 98 percent / NaH / tetrahydrofuran / 0.08 h / 0 °C
3: 96 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C
With
2,6-dimethylpyridine; tetrabutyl ammonium fluoride; sodium hydride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00049a022
