2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-chlorophenylimino)-methyl)-phenol

Base Information

• Chemical Name: 2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-chlorophenylimino)-methyl)-phenol
• CAS No.: 1401109-81-6
• Molecular Formula: C₄₇H₄₆ClNO
• Molecular Weight: 676.341
• Mol file: 1401109-81-6.mol

Synonyms:2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-chlorophenylimino)-methyl)-phenol

Chemical Property of 2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-chlorophenylimino)-methyl)-phenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-chlorophenylimino)-methyl)-phenol

There total 1 articles about 2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-chlorophenylimino)-methyl)-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

3,5-di-tert-butyl-2-hydroxybenzaldehyde (37942-07-7) + 2,6-bis(diphenylmethyl)-4-chloro-benzenamine (1373618-99-5) → 2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-chlorophenylimino)-methyl)-phenol (1401109-81-6)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 24h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1039/c5dt04408a

Reference yield: 84.0%

2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-chlorophenylimino)-methyl)-phenol (1401109-81-6) + trimethylaluminum (75-24-1) → dimethylaluminium 2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-chlorophenylimino)methyl)phenolate

Guidance literature:

In toluene; at -30 - 20 ℃;

DOI:10.1039/c2dt31215h

Reference yield:

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + 2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-chlorophenylimino)-methyl)-phenol (1401109-81-6) → [2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-chlorophenylimino)-methyl)-phenolato]Na*THF

Guidance literature:

With sodium hydride; Inert atmosphere; Glovebox;

DOI:10.1039/c5dt04408a

upstream raw materials:

3,5-di-tert-butyl-2-hydroxybenzaldehyde

2,6-bis(diphenylmethyl)-4-chloro-benzenamine