3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-dimethylmaleimido-β-D-glucopyranosyl-(1->4)-2-acetamido-1,6-anhydro-2-deoxy-β-D-glucopyranose

Base Information

Chemical Name:3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-dimethylmaleimido-β-D-glucopyranosyl-(1->4)-2-acetamido-1,6-anhydro-2-deoxy-β-D-glucopyranose
CAS No.:1143578-55-5
Molecular Formula:C₃₆H₄₀N₂O₁₂
Molecular Weight:692.72
Hs Code.:

Synonyms:3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-dimethylmaleimido-β-D-glucopyranosyl-(1->4)-2-acetamido-1,6-anhydro-2-deoxy-β-D-glucopyranose

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Chemical Property of 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-dimethylmaleimido-β-D-glucopyranosyl-(1->4)-2-acetamido-1,6-anhydro-2-deoxy-β-D-glucopyranose

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Technology Process of 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-dimethylmaleimido-β-D-glucopyranosyl-(1->4)-2-acetamido-1,6-anhydro-2-deoxy-β-D-glucopyranose

There total 1 articles about 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-dimethylmaleimido-β-D-glucopyranosyl-(1->4)-2-acetamido-1,6-anhydro-2-deoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 37042-50-5
2-acetamido-3-O-acetyl-1,6-anhydro-2-deoxy-β-D-glucopyranose

: 678159-04-1
2,2,2-Trichloro-acetimidic acid (2R,4aR,6S,7R,8R,8aS)-8-benzyloxy-7-(3,4-dimethyl-2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yl ester

: 1143578-55-5
3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-dimethylmaleimido-β-D-glucopyranosyl-(1->4)-2-acetamido-1,6-anhydro-2-deoxy-β-D-glucopyranose

Guidance literature:: 2-acetamido-3-O-acetyl-1,6-anhydro-2-deoxy-β-D-glucopyranose; 2,2,2-Trichloro-acetimidic acid (2R,4aR,6S,7R,8R,8aS)-8-benzyloxy-7-(3,4-dimethyl-2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yl ester; In dichloromethane; for 2h; Molecular sieve; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

Reference yield: 55.0%

: 1143578-55-5
3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-dimethylmaleimido-β-D-glucopyranosyl-(1->4)-2-acetamido-1,6-anhydro-2-deoxy-β-D-glucopyranose

: 108-24-7
acetic anhydride

: 1143578-67-9
2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-1,6-anhydro-2-deoxy-β-D-glucopyranose

Guidance literature:: 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-dimethylmaleimido-β-D-glucopyranosyl-(1->4)-2-acetamido-1,6-anhydro-2-deoxy-β-D-glucopyranose; With water; sodium hydroxide; In 1,4-dioxane; at 10 - 20 ℃; for 3h; pH=10 - 11; Inert atmosphere; Sonication;

With hydrogenchloride; water; In 1,4-dioxane; at 20 ℃; for 10h; pH=3;

acetic anhydride; With pyridine; at 20 ℃; for 20h;