(2S-cis)-2-(2-methyl-1-propenyl)-N-(4-nitrophenyl)-4-phenyl-3-oxazolidinecarboxamide

Base Information

• Chemical Name: (2S-cis)-2-(2-methyl-1-propenyl)-N-(4-nitrophenyl)-4-phenyl-3-oxazolidinecarboxamide
• CAS No.: 298210-07-8
• Molecular Formula: C₂₀H₂₁N₃O₄
• Molecular Weight: 367.404

Synonyms:(2S-cis)-2-(2-methyl-1-propenyl)-N-(4-nitrophenyl)-4-phenyl-3-oxazolidinecarboxamide

Chemical Property of (2S-cis)-2-(2-methyl-1-propenyl)-N-(4-nitrophenyl)-4-phenyl-3-oxazolidinecarboxamide

Chemical Property:

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Technology Process of (2S-cis)-2-(2-methyl-1-propenyl)-N-(4-nitrophenyl)-4-phenyl-3-oxazolidinecarboxamide

There total 3 articles about (2S-cis)-2-(2-methyl-1-propenyl)-N-(4-nitrophenyl)-4-phenyl-3-oxazolidinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3-dimethyl acrylaldehyde (107-86-8) → (2S-cis)-2-(2-methyl-1-propenyl)-N-(4-nitrophenyl)-4-phenyl-3-oxazolidinecarboxamide (298210-07-8)

Guidance literature:

Multi-step reaction with 2 steps

1: molecular sieves 4 Angstroem / CH₂Cl₂ / 3 h / 20 °C

2: 1.61 g / CH₂Cl₂ / 48 h / 20 °C

With 4 A molecular sieve; In dichloromethane;

DOI:10.1021/ja010463k

Reference yield:

(2S)-2-phenylglycinol (20989-17-7) → (2S-cis)-2-(2-methyl-1-propenyl)-N-(4-nitrophenyl)-4-phenyl-3-oxazolidinecarboxamide (298210-07-8)

Guidance literature:

Multi-step reaction with 2 steps

1: molecular sieves 4 Angstroem / CH₂Cl₂ / 3 h / 20 °C

2: 1.61 g / CH₂Cl₂ / 48 h / 20 °C

With 4 A molecular sieve; In dichloromethane;

DOI:10.1021/ja010463k

Reference yield:

4-Nitrophenyl isocyanate (100-28-7) + (2S,4S)-2-(2-Methyl-propenyl)-4-phenyl-oxazolidine → (2S-cis)-2-(2-methyl-1-propenyl)-N-(4-nitrophenyl)-4-phenyl-3-oxazolidinecarboxamide (298210-07-8)

Guidance literature:

In dichloromethane; at 20 ℃; for 48h;

DOI:10.1021/ja001113l

upstream raw materials:

4-Nitrophenyl isocyanate

3,3-dimethyl acrylaldehyde

(2S)-2-phenylglycinol

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