3-benzoyl-5-hydroxy-2-methyl-4,6-dinitrobenzofuran

Base Information

• Chemical Name: 3-benzoyl-5-hydroxy-2-methyl-4,6-dinitrobenzofuran
• CAS No.: 370872-63-2
• Molecular Formula: C₁₆H₁₀N₂O₇
• Molecular Weight: 342.265
• Mol file: 370872-63-2.mol

Synonyms:3-benzoyl-5-hydroxy-2-methyl-4,6-dinitrobenzofuran

Chemical Property of 3-benzoyl-5-hydroxy-2-methyl-4,6-dinitrobenzofuran

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 3-benzoyl-5-hydroxy-2-methyl-4,6-dinitrobenzofuran

There total 1 articles about 3-benzoyl-5-hydroxy-2-methyl-4,6-dinitrobenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.9%

2-methyl-3-benzoyl-5-hydroxybenzofuran (85992-24-1) → 3-benzoyl-5-hydroxy-2-methyl-4,6-dinitrobenzofuran (370872-63-2)

Guidance literature:

With nitric acid; In acetic acid; at 20 ℃; for 5h;

DOI:10.1007/BF02269537

Reference yield: 37.1%

N,N-dimethylformamide diethyl diacetal (1188-33-6) + 3-benzoyl-5-hydroxy-2-methyl-4,6-dinitrobenzofuran (370872-63-2) → 3-benzoyl-5-ethoxy-2-(β-dimethylaminovinyl)-4,6-dinitrobenzofuran (308797-03-7)

Guidance literature:

In N,N-dimethyl-formamide; for 5h; Heating;

DOI:10.1007/BF02269537

upstream raw materials:

2-methyl-3-benzoyl-5-hydroxybenzofuran

Downstream raw materials:

3-benzoyl-5-ethoxy-2-(β-dimethylaminovinyl)-4,6-dinitrobenzofuran