benzoyl cyanide azine

Base Information

• Chemical Name: benzoyl cyanide azine
• CAS No.: 57750-39-7
• Molecular Formula: C₁₆H₁₀N₄
• Molecular Weight: 258.282

Synonyms:benzoyl cyanide azine

Chemical Property of benzoyl cyanide azine

Chemical Property:

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Technology Process of benzoyl cyanide azine

There total 2 articles about benzoyl cyanide azine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

Bromo-ethylsulfanyl-phenyl-acetonitrile (65961-93-5) → benzoyl cyanide azine (57750-39-7)

Guidance literature:

With hydrazine; In acetonitrile;

DOI:10.1016/S0040-4039(01)81968-7

Reference yield: 13.0%

4-diazo-5-phenyl-4H-1,2,3-triazole (64781-77-7) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 4,5-Diphenyl-1H-[1,2,3]triazole (5533-73-3) + phenanthrene-9,10-dicarbonitrile (2510-54-5) + 7-cyano-7-phenylnorcaradiene (32777-15-4) + benzoyl cyanide azine (57750-39-7)

Guidance literature:

for 3h; Further byproducts given;

DOI:10.1016/S0040-4039(00)85773-1

Reference yield: 89.0%

benzoyl cyanide azine (57750-39-7) → Benzoic acid [1-cyano-1-phenyl-meth-(Z)-ylidene]-hydrazide (80403-30-1)

Guidance literature:

With sodium hydroxide; In dimethyl sulfoxide; for 0.166667h; Ambient temperature;

DOI:10.1016/S0040-4039(01)81968-7

upstream raw materials:

Bromo-ethylsulfanyl-phenyl-acetonitrile

4-diazo-5-phenyl-4H-1,2,3-triazole

benzene

Downstream raw materials:

Benzoic acid [1-cyano-1-phenyl-meth-(Z)-ylidene]-hydrazide

3,6-diphenyl-4H-[1,2,4]triazin-5-one

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