4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 2-benzyloxycarbonyl-3-[4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoyloxy]-2-methyl-propyl ester

Base Information

Chemical Name:4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 2-benzyloxycarbonyl-3-[4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoyloxy]-2-methyl-propyl ester
CAS No.:635703-94-5
Molecular Formula:C₆₀H₉₂O₈
Molecular Weight:941.386
Hs Code.:

4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[<i>a</i>]phenanthren-17-yl)-pentanoic acid 2-benzyloxycarbonyl-3-[4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[<i>a</i>]phenanthren-17-yl)-pentanoyloxy]-2-methyl-propyl ester

Synonyms:4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 2-benzyloxycarbonyl-3-[4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoyloxy]-2-methyl-propyl ester

Suppliers and Price of 4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 2-benzyloxycarbonyl-3-[4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoyloxy]-2-methyl-propyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 2-benzyloxycarbonyl-3-[4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoyloxy]-2-methyl-propyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 2-benzyloxycarbonyl-3-[4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoyloxy]-2-methyl-propyl ester

There total 2 articles about 4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 2-benzyloxycarbonyl-3-[4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoyloxy]-2-methyl-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 635703-92-3
4-(10,13-dimethyl-3-trifluoroacetoxy-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 2-benzyloxycarbonyl-3-[4-(10,13-dimethyl-3-trifluoroacetoxy-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoyloxy]-2-methyl-propyl ester

: 635703-94-5
4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 2-benzyloxycarbonyl-3-[4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoyloxy]-2-methyl-propyl ester

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; methanol; for 6h;
DOI:10.1055/s-2003-41041

Reference yield:

: 181633-71-6
3α-Trifluoroacetoxy-5β-cholan-24-oyl chloride

: 635703-94-5
4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 2-benzyloxycarbonyl-3-[4-(3-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoyloxy]-2-methyl-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / DMAP; Et₃N / CH₂Cl₂ / 49 h / 0 - 20 °C

2: 71 percent / aq. NaHCO₃ / methanol; tetrahydrofuran / 6 h

With dmap; sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1055/s-2003-41041