Technology Process of C25H38BN3O4Si
There total 5 articles about C25H38BN3O4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 4 steps
1: water; potassium hydroxide / methanol / 15 h / 20 °C
2: triethylamine / N,N-dimethyl-formamide / 15 h / 20 °C
3: ammonium acetate / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 120 °C
4: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 2 h / 100 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; ammonium acetate; water; potassium acetate; triethylamine; potassium hydroxide;
In
1,4-dioxane; methanol; 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride / water; methanol / 5 h / 20 °C
1.2: 7 h / 20 °C
1.3: 15 h / 20 °C
2.1: water; potassium hydroxide / methanol / 15 h / 20 °C
3.1: triethylamine / N,N-dimethyl-formamide / 15 h / 20 °C
4.1: ammonium acetate / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 120 °C
5.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 2 h / 100 °C / Inert atmosphere
With
hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; ammonium acetate; water; potassium acetate; triethylamine; potassium hydroxide;
In
1,4-dioxane; methanol; 5,5-dimethyl-1,3-cyclohexadiene; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / N,N-dimethyl-formamide / 15 h / 20 °C
2: ammonium acetate / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 120 °C
3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 2 h / 100 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; ammonium acetate; potassium acetate; triethylamine;
In
1,4-dioxane; 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl-formamide;