C₂₉H₄₁Cl₄N₂O₁₂P

Base Information

• Chemical Name: C₂₉H₄₁Cl₄N₂O₁₂P
• CAS No.: 259684-24-7
• Molecular Formula: C₂₉H₄₁Cl₄N₂O₁₂P
• Molecular Weight: 782.436
• Mol file: 259684-24-7.mol

Synonyms:C₂₉H₄₁Cl₄N₂O₁₂P

Chemical Property of C₂₉H₄₁Cl₄N₂O₁₂P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₄₁Cl₄N₂O₁₂P

There total 6 articles about C₂₉H₄₁Cl₄N₂O₁₂P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2R,3S,4S,5R,6S)-2-(acetoxymethyl)-6-(4-formylphenoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate (2887-07-2,31873-42-4,148579-45-7) → C29H41Cl4N2O12P (259684-24-7)

Guidance literature:

Multi-step reaction with 4 steps

1: 72 percent / NaBH₄ / CHCl₃; propan-2-ol

2: PCl₃; Et₃N

3: Et₃N

4: tert-butyl hydroperoxide

With tert.-butylhydroperoxide; sodium tetrahydroborate; triethylamine; phosphorus trichloride; In chloroform; isopropyl alcohol; 1: Reduction / 2: Substitution / 3: Substitution / 4: Oxidation;

DOI:10.1039/a907719g

Reference yield:

4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → C29H41Cl4N2O12P (259684-24-7)

Guidance literature:

Multi-step reaction with 5 steps

1: 73 percent / Ag₂O / acetonitrile / 8 h / 20 °C

2: 72 percent / NaBH₄ / CHCl₃; propan-2-ol

3: PCl₃; Et₃N

4: Et₃N

5: tert-butyl hydroperoxide

With tert.-butylhydroperoxide; sodium tetrahydroborate; triethylamine; silver(l) oxide; phosphorus trichloride; In chloroform; isopropyl alcohol; acetonitrile; 1: Substitution / 2: Reduction / 3: Substitution / 4: Substitution / 5: Oxidation;

DOI:10.1039/a907719g

Reference yield:

1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside (3068-32-4) → C29H41Cl4N2O12P (259684-24-7)

Guidance literature:

Multi-step reaction with 5 steps

1: 73 percent / Ag₂O / acetonitrile / 8 h / 20 °C

2: 72 percent / NaBH₄ / CHCl₃; propan-2-ol

3: PCl₃; Et₃N

4: Et₃N

5: tert-butyl hydroperoxide

With tert.-butylhydroperoxide; sodium tetrahydroborate; triethylamine; silver(l) oxide; phosphorus trichloride; In chloroform; isopropyl alcohol; acetonitrile; 1: Substitution / 2: Reduction / 3: Substitution / 4: Substitution / 5: Oxidation;

DOI:10.1039/a907719g

upstream raw materials:

(2R,3S,4S,5R,6S)-2-(acetoxymethyl)-6-(4-formylphenoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

4-hydroxy-benzaldehyde

(2R,3S,4S,5R,6S)-2-(acetoxymethyl)-6-(4-(hydroxymethyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside