C₁₉H₁₆BrNO₆S

Base Information

• Chemical Name: C₁₉H₁₆BrNO₆S
• CAS No.: 1333378-23-6
• Molecular Formula: C₁₉H₁₆BrNO₆S
• Molecular Weight: 466.309
• Mol file: 1333378-23-6.mol

Synonyms:C₁₉H₁₆BrNO₆S

Chemical Property of C₁₉H₁₆BrNO₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₉H₁₆BrNO₆S

There total 1 articles about C₁₉H₁₆BrNO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C12H10BrNO4 (1333378-22-5) + p-toluenesulfonyl chloride (98-59-9) → C19H16BrNO6S (1333378-23-6)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 ℃; for 2h;

DOI:10.1002/ejoc.201100242

Reference yield: 95.0%

C19H16BrNO6S (1333378-23-6) → C18H18BrNO5S (1333378-24-7)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃;

DOI:10.1002/ejoc.201100242

Reference yield:

C19H16BrNO6S (1333378-23-6) → C21H22BrNO5S (1333378-25-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 0 - 20 °C

2: camphor-10-sulfonic acid / dichloromethane / 0 - 20 °C

With sodium tetrahydroborate; camphor-10-sulfonic acid; In methanol; dichloromethane;

DOI:10.1002/ejoc.201100242

upstream raw materials:

C₁₂H₁₀BrNO₄

p-toluenesulfonyl chloride

Downstream raw materials:

C₂₄H₂₄BrNO₇S

C₃₅H₃₅N₃O₈S₂

C₁₈H₁₈BrNO₅S

C₂₁H₂₂BrNO₅S