Technology Process of C29H28O5
There total 9 articles about C29H28O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
methanol; diethyl ether; water;
for 6.5h;
Reflux;
Inert atmosphere;
DOI:10.1016/j.bmcl.2011.09.116
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 24 h / 110 °C / Inert atmosphere
2: AD-mix β; methanesulfonamide / tetrahydrofuran; water; tert-butyl alcohol / 120 h / 0 °C
3: hydrogenchloride / methanol; diethyl ether; water / 6.5 h / Reflux; Inert atmosphere
With
hydrogenchloride; methanesulfonamide; AD-mix β; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
tetrahydrofuran; methanol; diethyl ether; water; toluene; tert-butyl alcohol;
2: Sharpless dihydroxylation;
DOI:10.1016/j.bmcl.2011.09.116
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
2: bromine; triethylamine; triphenylphosphine / dichloromethane / 0 - 20 °C
3: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 24 h / 110 °C / Inert atmosphere
4: AD-mix β; methanesulfonamide / tetrahydrofuran; water; tert-butyl alcohol / 120 h / 0 °C
5: hydrogenchloride / methanol; diethyl ether; water / 6.5 h / Reflux; Inert atmosphere
With
hydrogenchloride; lithium aluminium tetrahydride; methanesulfonamide; AD-mix β; bromine; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; triphenylphosphine;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; tert-butyl alcohol;
4: Sharpless dihydroxylation;
DOI:10.1016/j.bmcl.2011.09.116
