4-methylphenyl 2,3-di-O-acetyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:4-methylphenyl 2,3-di-O-acetyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside
CAS No.:219518-20-4
Molecular Formula:C₂₄H₂₆O₇S
Molecular Weight:458.532
Hs Code.:

Synonyms:4-methylphenyl 2,3-di-O-acetyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Suppliers and Price of 4-methylphenyl 2,3-di-O-acetyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 5 raw suppliers

Chemical Property of 4-methylphenyl 2,3-di-O-acetyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Chemical Property:

Boiling Point:578.2±50.0 °C(Predicted)
Density:1.31±0.1 g/cm3(Predicted)

Purity/Quality:: 98%,99%, ^*data from raw suppliers

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Technology Process of 4-methylphenyl 2,3-di-O-acetyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

There total 8 articles about 4-methylphenyl 2,3-di-O-acetyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 108-24-7
acetic anhydride

: 219518-19-1
4-methylphenyl 4,6-O-benzylidene-1-thio-β-D-glucopyranoside

: 219518-20-4
4-methylphenyl 2,3-di-O-acetyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; dmap; at 0 ℃;

Reference yield: 85.0%

: 849834-73-7
(2S,3R,4S,5R)-5-hydroxy-6-(hydroxymethyl)-2-(p-tolylthio)tetrahydro-2H-pyran-3,4-diyldiacetate

: 1125-88-8
benzaldehyde dimethyl acetal

: 219518-20-4
4-methylphenyl 2,3-di-O-acetyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: With iron(III) chloride; In acetonitrile; at 20 ℃; for 2.5h;
DOI:10.1016/j.carres.2011.01.003

Reference yield: 75.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 1152-39-2
p-methylphenyl 1-thio-β-D-glucopyranoside

: 108-24-7
acetic anhydride

: 219518-20-4
4-methylphenyl 2,3-di-O-acetyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: benzaldehyde dimethyl acetal; p-methylphenyl 1-thio-β-D-glucopyranoside; With toluene-4-sulfonic acid; In acetonitrile; at 25 ℃; Inert atmosphere;

acetic anhydride; In acetonitrile; at 40 ℃; Inert atmosphere;
DOI:10.1055/s-0028-1087913