(1R,2S)-3-(tert-butyldimethylsilanyloxy)-2-dimethylamino-1-(4-nitrophenyl)propan-1-ol

Base Information

Chemical Name:(1R,2S)-3-(tert-butyldimethylsilanyloxy)-2-dimethylamino-1-(4-nitrophenyl)propan-1-ol
CAS No.:1127228-49-2
Molecular Formula:C₁₇H₃₀N₂O₄Si
Molecular Weight:354.522
Hs Code.:

Synonyms:(1R,2S)-3-(tert-butyldimethylsilanyloxy)-2-dimethylamino-1-(4-nitrophenyl)propan-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S)-3-(tert-butyldimethylsilanyloxy)-2-dimethylamino-1-(4-nitrophenyl)propan-1-ol

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Technology Process of (1R,2S)-3-(tert-butyldimethylsilanyloxy)-2-dimethylamino-1-(4-nitrophenyl)propan-1-ol

There total 1 articles about (1R,2S)-3-(tert-butyldimethylsilanyloxy)-2-dimethylamino-1-(4-nitrophenyl)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₄N₂O₅Si

: 1127228-49-2
(1R,2S)-3-(tert-butyldimethylsilanyloxy)-2-dimethylamino-1-(4-nitrophenyl)propan-1-ol

Guidance literature:: With methanol; potassium carbonate; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1002/adsc.200800761

Reference yield: 41.0%

: 1127228-49-2
(1R,2S)-3-(tert-butyldimethylsilanyloxy)-2-dimethylamino-1-(4-nitrophenyl)propan-1-ol

: 1127228-51-6
(1S,2R)-3-(tert-butyldimethylsilyloxy)-N₂,N₂-dimethyl-1-(4-nitrophenyl)propane-1,2-diamine

Guidance literature:: (1R,2S)-3-(tert-butyldimethylsilanyloxy)-2-dimethylamino-1-(4-nitrophenyl)propan-1-ol; With di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; triphenylphosphine; In tetrahydrofuran; at 0 - 50 ℃; Inert atmosphere;

With triphenylphosphine; In tetrahydrofuran; at 50 ℃; for 2h; Inert atmosphere;

With water; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/adsc.200800761