2,6-bis{2-[(tert-butyldiphenylsilyl)oxy]ethoxy}-9-[4,5-bis(5-chloropentylsulfanyl)-1,3-dithiol-2-ylidene]-10-[4,5-bis(2-cyanoethylsulfanyl)-1,3-dithiol-2-ylidene]-9,10-dihydroanthracene

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Chemical Name:2,6-bis{2-[(tert-butyldiphenylsilyl)oxy]ethoxy}-9-[4,5-bis(5-chloropentylsulfanyl)-1,3-dithiol-2-ylidene]-10-[4,5-bis(2-cyanoethylsulfanyl)-1,3-dithiol-2-ylidene]-9,10-dihydroanthracene
CAS No.:905588-87-6
Molecular Formula:C₇₂H₈₀Cl₂N₂O₄S₈Si₂
Molecular Weight:1421.04
Hs Code.:

2,6-bis{2-[(tert-butyldiphenylsilyl)oxy]ethoxy}-9-[4,5-bis(5-chloropentylsulfanyl)-1,3-dithiol-2-ylidene]-10-[4,5-bis(2-cyanoethylsulfanyl)-1,3-dithiol-2-ylidene]-9,10-dihydroanthracene

Synonyms:2,6-bis{2-[(tert-butyldiphenylsilyl)oxy]ethoxy}-9-[4,5-bis(5-chloropentylsulfanyl)-1,3-dithiol-2-ylidene]-10-[4,5-bis(2-cyanoethylsulfanyl)-1,3-dithiol-2-ylidene]-9,10-dihydroanthracene

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Chemical Property of 2,6-bis{2-[(tert-butyldiphenylsilyl)oxy]ethoxy}-9-[4,5-bis(5-chloropentylsulfanyl)-1,3-dithiol-2-ylidene]-10-[4,5-bis(2-cyanoethylsulfanyl)-1,3-dithiol-2-ylidene]-9,10-dihydroanthracene

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Technology Process of 2,6-bis{2-[(tert-butyldiphenylsilyl)oxy]ethoxy}-9-[4,5-bis(5-chloropentylsulfanyl)-1,3-dithiol-2-ylidene]-10-[4,5-bis(2-cyanoethylsulfanyl)-1,3-dithiol-2-ylidene]-9,10-dihydroanthracene

There total 3 articles about 2,6-bis{2-[(tert-butyldiphenylsilyl)oxy]ethoxy}-9-[4,5-bis(5-chloropentylsulfanyl)-1,3-dithiol-2-ylidene]-10-[4,5-bis(2-cyanoethylsulfanyl)-1,3-dithiol-2-ylidene]-9,10-dihydroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 2,6-bis{2-[(tert-butyldiphenylsilyl)oxy]ethoxy}-10-[4,5-bis(5-chloropentylsulfanyl)-1,3-dithiol-2-ylidene]anthracene-9(10H)-one

: 132765-35-6
4,5-bis((2-cyanoethyl)thio)-1,3-dithiole-2-thione

: 905588-87-6
2,6-bis{2-[(tert-butyldiphenylsilyl)oxy]ethoxy}-9-[4,5-bis(5-chloropentylsulfanyl)-1,3-dithiol-2-ylidene]-10-[4,5-bis(2-cyanoethylsulfanyl)-1,3-dithiol-2-ylidene]-9,10-dihydroanthracene

Guidance literature:: With triethyl phosphite; In xylene; at 125 ℃; for 4.5h;
DOI:10.1021/ja062358m

Reference yield:

: 193148-62-8
4,5-bis(5-chloropentylsulfanyl)-1,3-dithiole-2-thione

: 905588-87-6
2,6-bis{2-[(tert-butyldiphenylsilyl)oxy]ethoxy}-9-[4,5-bis(5-chloropentylsulfanyl)-1,3-dithiol-2-ylidene]-10-[4,5-bis(2-cyanoethylsulfanyl)-1,3-dithiol-2-ylidene]-9,10-dihydroanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / triethyl phosphite / xylene / 3.5 h / 125 °C

2: 57 percent / triethyl phosphite / xylene / 4.5 h / 125 °C

With triethyl phosphite; In xylene;
DOI:10.1021/ja062358m

Reference yield:

: 345915-46-0
2,6-bis(2-tercbutyldiphenylsilyloxyethyloxy)-9,10-anthraquinone

: 905588-87-6
2,6-bis{2-[(tert-butyldiphenylsilyl)oxy]ethoxy}-9-[4,5-bis(5-chloropentylsulfanyl)-1,3-dithiol-2-ylidene]-10-[4,5-bis(2-cyanoethylsulfanyl)-1,3-dithiol-2-ylidene]-9,10-dihydroanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / triethyl phosphite / xylene / 3.5 h / 125 °C

2: 57 percent / triethyl phosphite / xylene / 4.5 h / 125 °C

With triethyl phosphite; In xylene;
DOI:10.1021/ja062358m