dimethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphoniteborane

Base Information

Chemical Name:dimethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphoniteborane
CAS No.:1337878-55-3
Molecular Formula:C₁₅H₂₈BO₆P
Molecular Weight:346.168
Hs Code.:

Synonyms:dimethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphoniteborane

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Chemical Property of dimethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphoniteborane

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Technology Process of dimethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphoniteborane

There total 1 articles about dimethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphoniteborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1337529-84-6
dimethyl 3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphonite

: 1337878-55-3
dimethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphoniteborane

Guidance literature:: With dimethylsulfide borane complex; In diethyl ether; at 20 ℃; for 15h;
DOI:10.1021/ol2020175

Reference yield: 67.0%

: 1337878-55-3
dimethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphoniteborane

: 1337529-84-6
dimethyl 3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphonite

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In benzene; at 50 ℃; for 22h;
DOI:10.1021/ol2020175

Reference yield:

: 1337878-55-3
dimethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphoniteborane

: 1337529-94-8
C₅₉H₈₆N₁₁O₁₈P

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-diaza-bicyclo[2.2.2]octane / benzene / 22 h / 50 °C

2: dimethyl sulfoxide / 4 h / 20 °C / pH 8.2 / tris/HCl buffer

With 1,4-diaza-bicyclo[2.2.2]octane; In dimethyl sulfoxide; benzene; 2: Staudinger reaction;
DOI:10.1021/ol2020175