4-Benzoyl-9-fluoro-7H-benzanthracen-7-one-α-13C

Base Information

Chemical Name:4-Benzoyl-9-fluoro-7H-benzanthracen-7-one-α-13C
CAS No.:73368-37-3
Molecular Formula:C₂₄H₁₃FO₂
Molecular Weight:353.353
Hs Code.:

4-Benzoyl-9-fluoro-7H-benz<de>anthracen-7-one-α-13C

Synonyms:4-Benzoyl-9-fluoro-7H-benzanthracen-7-one-α-13C

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Chemical Property of 4-Benzoyl-9-fluoro-7H-benzanthracen-7-one-α-13C

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Technology Process of 4-Benzoyl-9-fluoro-7H-benzanthracen-7-one-α-13C

There total 3 articles about 4-Benzoyl-9-fluoro-7H-benzanthracen-7-one-α-13C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 73368-36-2
α-Phenyl-9-fluoro-7-oxo-7H-benzanthracene-4-acetonitrile-α-13C

: 73368-37-3
4-Benzoyl-9-fluoro-7H-benzanthracen-7-one-α-13C

Guidance literature:: With sodium dichromate; sodium acetate; In acetic acid; for 3h; Heating;
DOI:10.1021/jo01299a004

Reference yield:

: 61735-79-3
9-Fluorobenzanthrone

: 73368-37-3
4-Benzoyl-9-fluoro-7H-benzanthracen-7-one-α-13C

Guidance literature:: Multi-step reaction with 2 steps

1: Potassium hydroxide / propan-2-ol / 4 h / 45 - 50 °C

2: 80 percent / Sodium acetate, sodium dichromate / acetic acid / 3 h / Heating

With potassium hydroxide; sodium dichromate; sodium acetate; In acetic acid; isopropyl alcohol;
DOI:10.1021/jo01299a004

Reference yield:

: 73368-35-1
<α-13C>Benzolacetonitril

: 73368-37-3
4-Benzoyl-9-fluoro-7H-benzanthracen-7-one-α-13C

Guidance literature:: Multi-step reaction with 2 steps

1: Potassium hydroxide / propan-2-ol / 4 h / 45 - 50 °C

2: 80 percent / Sodium acetate, sodium dichromate / acetic acid / 3 h / Heating

With potassium hydroxide; sodium dichromate; sodium acetate; In acetic acid; isopropyl alcohol;
DOI:10.1021/jo01299a004