methoxymethyl O-(3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

Base Information

Chemical Name:methoxymethyl O-(3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside
CAS No.:880480-63-7
Molecular Formula:C₅₆H₆₂O₁₂
Molecular Weight:927.101
Hs Code.:

Synonyms:methoxymethyl O-(3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

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Chemical Property of methoxymethyl O-(3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

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Technology Process of methoxymethyl O-(3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

There total 5 articles about methoxymethyl O-(3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.8%

: 880480-61-5
methoxymethyl O-(1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

: 880480-63-7
methoxymethyl O-(3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 3h;
DOI:10.3987/COM-05-S(K)54

Reference yield:

: 880480-38-6
1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranose

: 880480-63-7
methoxymethyl O-(3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 81.8 percent / diethylaminosulfur trifluoride / CH₂Cl₂ / 1 h / 20 °C

2: 57.2 percent / zirconocene dichloride; 4 Angstroem molecular sieves; AgClO₄ / CH₂Cl₂ / 2.5 h / 20 °C

3: 90.8 percent / NaOMe / methanol / 3 h / 20 °C

With diethylamino-sulfur trifluoride; 4 A molecular sieve; zirconocene dichloride; sodium methylate; silver perchlorate; In methanol; dichloromethane;
DOI:10.3987/COM-05-S(K)54

Reference yield:

: 880480-39-7
1-O-acetyl-3,4,5-tri-O-benzyl-β-D-fructopyranosyl fluoride

: 880480-63-7
methoxymethyl O-(3,4,5-tri-O-benzyl-β-D-fructopyranosyl)-(2->1)-3,4,5-tri-O-benzyl-β-D-fructopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 57.2 percent / zirconocene dichloride; 4 Angstroem molecular sieves; AgClO₄ / CH₂Cl₂ / 2.5 h / 20 °C

2: 90.8 percent / NaOMe / methanol / 3 h / 20 °C

With 4 A molecular sieve; zirconocene dichloride; sodium methylate; silver perchlorate; In methanol; dichloromethane;
DOI:10.3987/COM-05-S(K)54