1,3-bis(2,6-dimethylphenyl)-2-iodo-2,3-dihydro-1H-1,3,2-diazaborol0e

Base Information

Chemical Name:1,3-bis(2,6-dimethylphenyl)-2-iodo-2,3-dihydro-1H-1,3,2-diazaborol0e
CAS No.:212375-84-3
Molecular Formula:C₁₈H₂₀BIN₂
Molecular Weight:402.086
Hs Code.:

Synonyms:1,3-bis(2,6-dimethylphenyl)-2-iodo-2,3-dihydro-1H-1,3,2-diazaborol0e

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Chemical Property of 1,3-bis(2,6-dimethylphenyl)-2-iodo-2,3-dihydro-1H-1,3,2-diazaborol0e

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Technology Process of 1,3-bis(2,6-dimethylphenyl)-2-iodo-2,3-dihydro-1H-1,3,2-diazaborol0e

There total 1 articles about 1,3-bis(2,6-dimethylphenyl)-2-iodo-2,3-dihydro-1H-1,3,2-diazaborol0e which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: glyoxalbis(2,6-dimethylphenylimine)

: 13517-10-7
boron triiodide

: 212375-84-3
1,3-bis(2,6-dimethylphenyl)-2-iodo-2,3-dihydro-1H-1,3,2-diazaborol0e

Guidance literature:: In hexane; dichloromethane; Ar atmosphere, addn. of CH2Cl2 soln. of 1,4-diazabutadiene and n-hexane soln. of BCl3 into a mixture of n-hexane and CH2Cl2 at -10°C, filtration, warming to room temp., stirring ( 5 d); filtration, concn. to dryness, extn. (n-hexane), decantation, concn. of combined filtrates, crystn. (-4°C, 3 d), sublimation (380°C, 0.01 Torr); elem. anal.;
DOI:10.1002/(SICI)1099-0682(199808)1998:8<1145::AID-EJIC1145>3.0.CO;2-H

Reference yield: 93.0%

: 1701-93-5
silver thiocyanate

: 212375-84-3
1,3-bis(2,6-dimethylphenyl)-2-iodo-2,3-dihydro-1H-1,3,2-diazaborol0e

: 212375-89-8
C₁₉H₂₀BN₃S

Guidance literature:: In acetonitrile; byproducts: AgI; Ar atmosphere, addn. of AgSCN to a slurry of diazaborole in CH3CN, stirring (20°C, 5 h); filtration, concn. to dryness, extn. (n-hexane), filtration, removement of volatiles; elem. anal.;
DOI:10.1002/(SICI)1099-0682(199808)1998:8<1145::AID-EJIC1145>3.0.CO;2-H

Reference yield: 89.0%

: 212375-84-3
1,3-bis(2,6-dimethylphenyl)-2-iodo-2,3-dihydro-1H-1,3,2-diazaborol0e

: 1,3-bis(2,6-dimethylphenyl)-2,3-dihydro-1H-1,3,2-diazaborole

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 0.0833333h; Ambient temperature;
DOI:10.1002/(SICI)1099-0682(199903)1999:3<491::AID-EJIC491>3.0.CO;2-9