1-chloro-1-(thiophenoxy)-1H-cyclobutanaphthalene

Base Information

Chemical Name:1-chloro-1-(thiophenoxy)-1H-cyclobutanaphthalene
CAS No.:85925-09-3
Molecular Formula:C₁₇H₁₁ClS
Molecular Weight:282.793
Hs Code.:

1-chloro-1-(thiophenoxy)-1H-cyclobuta<de>naphthalene

Synonyms:1-chloro-1-(thiophenoxy)-1H-cyclobutanaphthalene

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Chemical Property of 1-chloro-1-(thiophenoxy)-1H-cyclobutanaphthalene

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Technology Process of 1-chloro-1-(thiophenoxy)-1H-cyclobutanaphthalene

There total 6 articles about 1-chloro-1-(thiophenoxy)-1H-cyclobutanaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 85924-90-9
1-(thiophenoxy)-1H-cyclobutanaphthalene

: 85925-09-3
1-chloro-1-(thiophenoxy)-1H-cyclobutanaphthalene

Guidance literature:: With N-chloro-succinimide; In tetrachloromethane; for 12h; Heating;
DOI:10.1021/ja00357a022

Reference yield:

: 54125-11-0
1-Bromo-1H-cyclobutanaphthalene

: 85925-09-3
1-chloro-1-(thiophenoxy)-1H-cyclobutanaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent Turnov_. / sodium methoxide / ethanol / 48 h / Heating

2: 93 percent / N-chlorosuccinimide / CCl₄ / 12 h / Heating

With N-chloro-succinimide; sodium methylate; In tetrachloromethane; ethanol;
DOI:10.1021/ja00357a022

Reference yield:

: 24973-91-9
1H-Cyclobutanaphthalene

: 85925-09-3
1-chloro-1-(thiophenoxy)-1H-cyclobutanaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 4.5 h / Heating

2: 83 percent Turnov_. / sodium methoxide / ethanol / 48 h / Heating

3: 93 percent / N-chlorosuccinimide / CCl₄ / 12 h / Heating

With N-chloro-succinimide; N-Bromosuccinimide; Perbenzoic acid; sodium methylate; In tetrachloromethane; ethanol;
DOI:10.1021/ja00357a022