(η5-cyclopentadienyl)((η5-cyclopentadienyl)ethenecobalt)-μ-(η4-2,4-di-tert-butyl-1,3-diphosphacyclobutadiene)cobalt

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Chemical Name:(η5-cyclopentadienyl)((η5-cyclopentadienyl)ethenecobalt)-μ-(η4-2,4-di-tert-butyl-1,3-diphosphacyclobutadiene)cobalt
CAS No.:109885-86-1
Molecular Formula:C₂₂H₃₂Co₂P₂
Molecular Weight:476.43
Hs Code.:

Synonyms:(η5-cyclopentadienyl)((η5-cyclopentadienyl)ethenecobalt)-μ-(η4-2,4-di-tert-butyl-1,3-diphosphacyclobutadiene)cobalt

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Chemical Property of (η5-cyclopentadienyl)((η5-cyclopentadienyl)ethenecobalt)-μ-(η4-2,4-di-tert-butyl-1,3-diphosphacyclobutadiene)cobalt

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Technology Process of (η5-cyclopentadienyl)((η5-cyclopentadienyl)ethenecobalt)-μ-(η4-2,4-di-tert-butyl-1,3-diphosphacyclobutadiene)cobalt

There total 2 articles about (η5-cyclopentadienyl)((η5-cyclopentadienyl)ethenecobalt)-μ-(η4-2,4-di-tert-butyl-1,3-diphosphacyclobutadiene)cobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: η5-cyclopentadienylbis(ethene)cobalt

: 78129-68-7
2,2-dimethylpropylidynephosphine

: 109885-86-1
(η5-cyclopentadienyl)((η5-cyclopentadienyl)ethenecobalt)-μ-(η4-2,4-di-tert-butyl-1,3-diphosphacyclobutadiene)cobalt

Guidance literature:: In diethyl ether; pentane; byproducts: C2H4; Ar atmosphere; dropwise addn. of PCC(CH3)3 (4.0 mmol) in ether/pentane to a soln. of the Co complex (3.7 mmol) in ether/pentane at -30°C; mixt. was kept at -5°C for 1 h;; evapn.; residue was dissolved in pentane; filtration through Florisil; filtrate was cooled at -78°C for 12 h; removal of solvent; dryingat 1E-3 torr; elem. anal.;;