C₁₈H₁₅BrN₂O₂S

Base Information

Chemical Name:C₁₈H₁₅BrN₂O₂S
CAS No.:1423703-65-4
Molecular Formula:C₁₈H₁₅BrN₂O₂S
Molecular Weight:403.299
Hs Code.:

C<sub>18</sub>H<sub>15</sub>BrN<sub>2</sub>O<sub>2</sub>S

Synonyms:C₁₈H₁₅BrN₂O₂S

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Chemical Property of C₁₈H₁₅BrN₂O₂S

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Technology Process of C₁₈H₁₅BrN₂O₂S

There total 4 articles about C₁₈H₁₅BrN₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1517-69-7
(R)-1-phenylethanol

: 900587-78-2
C₁₀H₆BrNO₂S

: 1423703-65-4
C₁₈H₁₅BrN₂O₂S

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In toluene; at 80 ℃; for 3h;

Reference yield:

: 834885-05-1
ethyl 2-amino-4-(4-bromophenyl)thiazole-5-carboxylate

: 1423703-65-4
C₁₈H₁₅BrN₂O₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: hypophosphorous acid; sodium nitrite / water / 0 - 25 °C

2.1: water; sodium hydroxide / methanol / 3 h / 20 °C

2.2: pH Ca_. 3

3.1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 80 °C

With diphenyl phosphoryl azide; water; hypophosphorous acid; triethylamine; sodium hydroxide; sodium nitrite; In methanol; water; toluene;

Reference yield:

: 87943-97-3
ethyl 2-bromo-3-(4-bromophenyl)-3-oxopropanoate

: 1423703-65-4
C₁₈H₁₅BrN₂O₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethanol / 2 h / 75 °C

2.1: hypophosphorous acid; sodium nitrite / water / 0 - 25 °C

3.1: water; sodium hydroxide / methanol / 3 h / 20 °C

3.2: pH Ca_. 3

4.1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 80 °C

With diphenyl phosphoryl azide; water; hypophosphorous acid; triethylamine; sodium hydroxide; sodium nitrite; In methanol; ethanol; water; toluene;