N-2-furoylalanine 4-tert-butylbenzyl thioester

Base Information

Chemical Name:N-2-furoylalanine 4-tert-butylbenzyl thioester
CAS No.:1361143-30-7
Molecular Formula:C₁₉H₂₃NO₃S
Molecular Weight:345.463
Hs Code.:

Synonyms:N-2-furoylalanine 4-tert-butylbenzyl thioester

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Chemical Property of N-2-furoylalanine 4-tert-butylbenzyl thioester

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Technology Process of N-2-furoylalanine 4-tert-butylbenzyl thioester

There total 3 articles about N-2-furoylalanine 4-tert-butylbenzyl thioester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1361143-05-6
N-2-furoylalanine azlactone

: 49543-63-7
4-tert-butylbenzyl mercaptan

: 1361143-30-7
N-2-furoylalanine 4-tert-butylbenzyl thioester

: 1361143-08-9
N-2-furoylalanine 4-tert-butylbenzyl thioester

Guidance literature:: With Bis-QN-SQA; In dichloromethane; at 20 ℃; for 20h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/jo202662d

Reference yield:

: 1001616-79-0
N-2-furoylalanine

: 1361143-30-7
N-2-furoylalanine 4-tert-butylbenzyl thioester

: 1361143-08-9
N-2-furoylalanine 4-tert-butylbenzyl thioester

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide / dichloromethane / 20 °C / Inert atmosphere

2: (8S,9R)-6'-methoxy-9-(1-hydroxynaphtalen-2-yl)-cinchonan / dichloromethane / 72 h / 19 - 21 °C / Inert atmosphere

With (8S,9R)-6'-methoxy-9-(1-hydroxynaphtalen-2-yl)-cinchonan; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jo202662d

Reference yield:

: 527-69-5
2-furancarbonyl chloride

: 1361143-30-7
N-2-furoylalanine 4-tert-butylbenzyl thioester

: 1361143-08-9
N-2-furoylalanine 4-tert-butylbenzyl thioester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / water / 0 - 20 °C

2: dicyclohexyl-carbodiimide / dichloromethane / 20 °C / Inert atmosphere

3: (8S,9R)-6'-methoxy-9-(1-hydroxynaphtalen-2-yl)-cinchonan / dichloromethane / 72 h / 19 - 21 °C / Inert atmosphere

With (8S,9R)-6'-methoxy-9-(1-hydroxynaphtalen-2-yl)-cinchonan; dicyclohexyl-carbodiimide; sodium hydroxide; In dichloromethane; water;
DOI:10.1021/jo202662d