Technology Process of C24H34N2O6
There total 10 articles about C24H34N2O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium on carbon; hydrogen;
In
ethanol;
at 60 ℃;
under 760.051 Torr;
DOI:10.1021/ol301331t
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: water; toluene-4-sulfonic acid / acetone / 24 h / 70 °C
2.1: potassium hydroxide / dimethyl sulfoxide / 2 h / 25 °C / Inert atmosphere
3.1: sodium tetrahydroborate / ethanol / 2 h / 25 °C
4.1: pyridine; 3-chloro-benzenecarboperoxoic acid / hexane; dichloromethane / -30 - 20 °C
5.1: chlorosulfonic acid / dichloromethane / 6 h / -30 °C
6.1: lithium diisopropyl amide / tetrahydrofuran / 0.53 h / -78 - 0 °C
6.2: 0.17 h
6.3: 7 h
7.1: palladium on carbon; hydrogen / ethanol / 60 °C / 760.05 Torr
With
pyridine; chlorosulfonic acid; sodium tetrahydroborate; palladium on carbon; water; hydrogen; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; lithium diisopropyl amide;
In
tetrahydrofuran; ethanol; hexane; dichloromethane; dimethyl sulfoxide; acetone;
5.1: Schmidt reaction;
DOI:10.1021/ol301331t
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium tetrahydroborate / ethanol / 2 h / 25 °C
2.1: pyridine; 3-chloro-benzenecarboperoxoic acid / hexane; dichloromethane / -30 - 20 °C
3.1: chlorosulfonic acid / dichloromethane / 6 h / -30 °C
4.1: lithium diisopropyl amide / tetrahydrofuran / 0.53 h / -78 - 0 °C
4.2: 0.17 h
4.3: 7 h
5.1: palladium on carbon; hydrogen / ethanol / 60 °C / 760.05 Torr
With
pyridine; chlorosulfonic acid; sodium tetrahydroborate; palladium on carbon; hydrogen; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide;
In
tetrahydrofuran; ethanol; hexane; dichloromethane;
3.1: Schmidt reaction;
DOI:10.1021/ol301331t
