[5,10,15-tris(trifluoromethyl)corrolato](triphenylphosphine)cobalt(III)

Base Information

Chemical Name:[5,10,15-tris(trifluoromethyl)corrolato](triphenylphosphine)cobalt(III)
CAS No.:1272377-66-8
Molecular Formula:C₄₀H₂₃CoF₉N₄P
Molecular Weight:820.602
Hs Code.:

Synonyms:[5,10,15-tris(trifluoromethyl)corrolato](triphenylphosphine)cobalt(III)

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Chemical Property of [5,10,15-tris(trifluoromethyl)corrolato](triphenylphosphine)cobalt(III)

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Technology Process of [5,10,15-tris(trifluoromethyl)corrolato](triphenylphosphine)cobalt(III)

There total 2 articles about [5,10,15-tris(trifluoromethyl)corrolato](triphenylphosphine)cobalt(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.4%

: 5,10,15-tris(trifluoromethyl)corrole

: 603-35-0
triphenylphosphine

: 1272377-66-8
[5,10,15-tris(trifluoromethyl)corrolato](triphenylphosphine)cobalt(III)

Guidance literature:: 5,10,15-tris(trifluoromethyl)corrole; With sodium acetate; In ethanol; for 0.0833333h;

triphenylphosphine; With cobalt(II) diacetate tetrahydrate; In ethanol; for 0.333333h;
DOI:10.1021/ic1017032

Reference yield: 71.4%

: 5,10,15-tris(trifluoromethyl)corrole

: 6147-53-1
cobalt(II) diacetate tetrahydrate

: 603-35-0
triphenylphosphine

: 1272377-66-8
[5,10,15-tris(trifluoromethyl)corrolato](triphenylphosphine)cobalt(III)

Guidance literature:: With sodium acetate; In ethanol; corrole and AcONa were dissolved in abs. EtOH, stirred for 5 min, Co(OAc)2*4H2O and PPh3 were added, stirred for 20 min; react. mixt. was evapd., residue was chromd. on silica (n-hexane - CH2Cl2 95:5); elem. anal.;
DOI:10.1021/ic1017032