6-(4-bromo-2,5-dichlorophenoxy)hexyltrifluoromethanesulfonate

Base Information

• Chemical Name: 6-(4-bromo-2,5-dichlorophenoxy)hexyltrifluoromethanesulfonate
• CAS No.: 1638612-07-3
• Molecular Formula: C₁₃H₁₄BrCl₂F₃O₄S
• Molecular Weight: 474.123
• Mol file: 1638612-07-3.mol

Synonyms:6-(4-bromo-2,5-dichlorophenoxy)hexyltrifluoromethanesulfonate

Chemical Property of 6-(4-bromo-2,5-dichlorophenoxy)hexyltrifluoromethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 6-(4-bromo-2,5-dichlorophenoxy)hexyltrifluoromethanesulfonate

There total 1 articles about 6-(4-bromo-2,5-dichlorophenoxy)hexyltrifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trifluoromethylsulfonic anhydride (358-23-6) + 1-bromo-2,5-dichloro-4-[(6-hydroxyhexyl)oxy]benzene (1638612-00-6) → 6-(4-bromo-2,5-dichlorophenoxy)hexyltrifluoromethanesulfonate (1638612-07-3)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at -78 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1002/anie.201402238

Reference yield: 97.0%

6-(4-bromo-2,5-dichlorophenoxy)hexyltrifluoromethanesulfonate (1638612-07-3) → 1-bromo-2,5-dichloro-4-[(6-fluorohexyl)oxy] (1638612-19-7)

Guidance literature:

With potassium fluoride; 2,6-diisopropylphenyl; In 1,4-dioxane; at 45 ℃; for 1h; chemoselective reaction; Inert atmosphere; Glovebox;

DOI:10.1002/anie.201402238

upstream raw materials:

trifluoromethylsulfonic anhydride

1-bromo-2,5-dichloro-4-[(6-hydroxyhexyl)oxy]benzene

Downstream raw materials:

1-bromo-2,5-dichloro-4-[(6-fluorohexyl)oxy]