N⁴-benzoyl-5'-O-levulinoyl-2'-deoxycytidine-3'-O-dichlorophosphoridate

Base Information

• Chemical Name: N⁴-benzoyl-5'-O-levulinoyl-2'-deoxycytidine-3'-O-dichlorophosphoridate
• CAS No.: 1570197-35-1
• Molecular Formula: C₂₁H₂₂Cl₂N₃O₈P
• Molecular Weight: 546.301

Synonyms:N⁴-benzoyl-5'-O-levulinoyl-2'-deoxycytidine-3'-O-dichlorophosphoridate

Chemical Property of N⁴-benzoyl-5'-O-levulinoyl-2'-deoxycytidine-3'-O-dichlorophosphoridate

Chemical Property:

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Technology Process of N⁴-benzoyl-5'-O-levulinoyl-2'-deoxycytidine-3'-O-dichlorophosphoridate

There total 1 articles about N⁴-benzoyl-5'-O-levulinoyl-2'-deoxycytidine-3'-O-dichlorophosphoridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N4-benzoyl-5'-O-levulinoyl-2'-deoxycytidine → N4-benzoyl-5'-O-levulinoyl-2'-deoxycytidine-3'-O-dichlorophosphoridate (1570197-35-1)

Guidance literature:

With trimethyl phosphite; tributyl-amine; trichlorophosphate; at 0 - 20 ℃; for 0.966667h;

DOI:10.1016/j.tetlet.2014.01.077

Reference yield:

N4-benzoyl-5'-O-levulinoyl-2'-deoxycytidine-3'-O-dichlorophosphoridate (1570197-35-1) → N4-benzoyl-5-O-levulinoyl-2-deoxycytidine-3-O-tetraphosphate

Guidance literature:

With tributyl-amine; tris-(tri-n-butylammonium) triphosphate; In acetonitrile; at 20 ℃; for 0.333333h;

DOI:10.1080/15257770.2014.955193

Reference yield:

N4-benzoyl-5'-O-levulinoyl-2'-deoxycytidine-3'-O-dichlorophosphoridate (1570197-35-1) + triethylamine carbonate (15715-58-9) → C21H26N3O16P3*4C6H15N

Guidance literature:

N⁴-benzoyl-5'-O-levulinoyl-2'-deoxycytidine-3'-O-dichlorophosphoridate; With tributyl-amine; bis(tri-n-butylammonium) pyrophosphate; In acetonitrile; at 20 ℃;

triethylamine carbonate; In water; pH=5.5;

DOI:10.1016/j.tetlet.2014.01.077

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