11-naphthalen-2-yl-9-(toluene-4-sulfonyl)-9,10-dihydro-8H-9-azacyclopenta[b]phenanthrene

Base Information

Chemical Name:11-naphthalen-2-yl-9-(toluene-4-sulfonyl)-9,10-dihydro-8H-9-azacyclopenta[b]phenanthrene
CAS No.:1617506-56-5
Molecular Formula:C₃₃H₂₅NO₂S
Molecular Weight:499.633
Hs Code.:

Synonyms:11-naphthalen-2-yl-9-(toluene-4-sulfonyl)-9,10-dihydro-8H-9-azacyclopenta[b]phenanthrene

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Chemical Property of 11-naphthalen-2-yl-9-(toluene-4-sulfonyl)-9,10-dihydro-8H-9-azacyclopenta[b]phenanthrene

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Technology Process of 11-naphthalen-2-yl-9-(toluene-4-sulfonyl)-9,10-dihydro-8H-9-azacyclopenta[b]phenanthrene

There total 2 articles about 11-naphthalen-2-yl-9-(toluene-4-sulfonyl)-9,10-dihydro-8H-9-azacyclopenta[b]phenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1617506-65-6
C₃₃H₂₅NO₂S

: 1617506-56-5
11-naphthalen-2-yl-9-(toluene-4-sulfonyl)-9,10-dihydro-8H-9-azacyclopenta[b]phenanthrene

Guidance literature:: With aluminum oxide; In dichloromethane; at 130 ℃; Green chemistry;
DOI:10.1016/j.tetlet.2014.05.033

Reference yield: 84.0%

: 580-13-2
2-bromonaphthalene

: 18773-54-1
4-methyl-N,N-diprop-2-ynylbenzenesulfonamide

: 1617506-56-5
11-naphthalen-2-yl-9-(toluene-4-sulfonyl)-9,10-dihydro-8H-9-azacyclopenta[b]phenanthrene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 110 ℃; for 8h;
DOI:10.1016/j.tetlet.2015.02.093