Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-α-L-erythro-hexopyranosid-4-ulose

Base Information

Chemical Name:Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-α-L-erythro-hexopyranosid-4-ulose
CAS No.:109978-55-4
Molecular Formula:C₁₅H₁₉NO₅
Molecular Weight:293.32
Hs Code.:

Synonyms:Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-α-L-erythro-hexopyranosid-4-ulose

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Chemical Property of Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-α-L-erythro-hexopyranosid-4-ulose

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Technology Process of Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-α-L-erythro-hexopyranosid-4-ulose

There total 11 articles about Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-α-L-erythro-hexopyranosid-4-ulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 83532-10-9
methyl 3-(N-benzyloxycarbonylamino)-2,3,6-trideoxy-α-D-arabino-hexopyranoside

: 83532-11-0,109978-55-4
methyl 3-(benzyloxycarbonyl)amino-2,3,6-trideoxy-α-arabino-hexopyranosid-4-ulose

Guidance literature:: With dimethyl sulfoxide; trifluoroacetic anhydride; In dichloromethane; at -78 - -65 ℃; for 1.5h;
DOI:10.1248/cpb.39.2201

Reference yield: 91.0%

: 87357-51-5
Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-α-L-ribo-hexopyranosid

: 109978-55-4
Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-α-L-erythro-hexopyranosid-4-ulose

Guidance literature:: With pyridine; chromium(VI) oxide; acetic anhydride; In dichloromethane; for 0.333333h;

Reference yield:

: 18933-62-5
methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-α-D-arabino-hexopyranoside

: 83532-11-0,109978-55-4
methyl 3-(benzyloxycarbonyl)amino-2,3,6-trideoxy-α-arabino-hexopyranosid-4-ulose

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) H₂, triethylamine / 1.) Raney nickel / 1.) methanol, 2.) methanol, 3.) methanol

2: 93 percent / dimethylsulfoxide-trifluoracetic anhydride / CH₂Cl₂ / -65 °C

With hydrogen; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; nickel; In dichloromethane;
DOI:10.1248/cpb.30.1929