2-[2-allyloxy-5-(1,1,3,3-tetramethyl-butyl)-phenyl]-5-trifluoromethyl-2H-benzotriazole

Base Information

• Chemical Name: 2-[2-allyloxy-5-(1,1,3,3-tetramethyl-butyl)-phenyl]-5-trifluoromethyl-2H-benzotriazole
• CAS No.: 782477-37-6
• Molecular Formula: C₂₄H₂₈F₃N₃O
• Molecular Weight: 431.501
• Mol file: 782477-37-6.mol

Synonyms:2-[2-allyloxy-5-(1,1,3,3-tetramethyl-butyl)-phenyl]-5-trifluoromethyl-2H-benzotriazole

Chemical Property of 2-[2-allyloxy-5-(1,1,3,3-tetramethyl-butyl)-phenyl]-5-trifluoromethyl-2H-benzotriazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-[2-allyloxy-5-(1,1,3,3-tetramethyl-butyl)-phenyl]-5-trifluoromethyl-2H-benzotriazole

There total 1 articles about 2-[2-allyloxy-5-(1,1,3,3-tetramethyl-butyl)-phenyl]-5-trifluoromethyl-2H-benzotriazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

allyl bromide (106-95-6) + 5-Trifluoromethyl-2-(2-hydroxy-5-tert-octylphenyl)-2H-benzotriazole (207738-93-0) → 2-[2-allyloxy-5-(1,1,3,3-tetramethyl-butyl)-phenyl]-5-trifluoromethyl-2H-benzotriazole (782477-37-6)

Guidance literature:

5-Trifluoromethyl-2-(2-hydroxy-5-tert-octylphenyl)-2H-benzotriazole; With potassium hydroxide; In ethanol; at 20 ℃; for 2h;

allyl bromide; With potassium iodide; In ethanol; at 85 ℃; for 4.5h;

DOI:10.1021/jp021000j

Reference yield: 86.0%

2-[2-allyloxy-5-(1,1,3,3-tetramethyl-butyl)-phenyl]-5-trifluoromethyl-2H-benzotriazole (782477-37-6) → 5-(trifluoromethyl)-2-(2-hydroxy-3-allyl-5-tert-octylphenyl)-2H-benzotriazole (286471-15-6)

Guidance literature:

at 190 - 195 ℃; for 5h;

DOI:10.1021/jp021000j

upstream raw materials:

allyl bromide

5-Trifluoromethyl-2-(2-hydroxy-5-tert-octylphenyl)-2H-benzotriazole

Downstream raw materials:

5-(trifluoromethyl)-2-(2-hydroxy-3-allyl-5-tert-octylphenyl)-2H-benzotriazole