(S)-1-chloro-3-(4-(9-(4-((R)-2-hydroxy-3-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)propoxy)phenyl)-9H-fluoren-9-yl)phenoxy)propan-2-ol

Base Information

Chemical Name:(S)-1-chloro-3-(4-(9-(4-((R)-2-hydroxy-3-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)propoxy)phenyl)-9H-fluoren-9-yl)phenoxy)propan-2-ol
CAS No.:1403963-55-2
Molecular Formula:C₃₇H₄₁ClO₈
Molecular Weight:649.181
Hs Code.:

Synonyms:(S)-1-chloro-3-(4-(9-(4-((R)-2-hydroxy-3-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)propoxy)phenyl)-9H-fluoren-9-yl)phenoxy)propan-2-ol

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Chemical Property of (S)-1-chloro-3-(4-(9-(4-((R)-2-hydroxy-3-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)propoxy)phenyl)-9H-fluoren-9-yl)phenoxy)propan-2-ol

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Technology Process of (S)-1-chloro-3-(4-(9-(4-((R)-2-hydroxy-3-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)propoxy)phenyl)-9H-fluoren-9-yl)phenoxy)propan-2-ol

There total 3 articles about (S)-1-chloro-3-(4-(9-(4-((R)-2-hydroxy-3-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)propoxy)phenyl)-9H-fluoren-9-yl)phenoxy)propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1403963-70-1
(S)-1-chloro-3-(4-(9-(4-((R)-oxiran-2-ylmethoxy)phenyl)-9H-fluoren-9-yl)phenoxy)propan-2-ol

: 112-27-6
2,2'-[1,2-ethanediylbis(oxy)]bisethanol

: 1403963-55-2
(S)-1-chloro-3-(4-(9-(4-((R)-2-hydroxy-3-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)propoxy)phenyl)-9H-fluoren-9-yl)phenoxy)propan-2-ol

Guidance literature:: bismuth(lll) trifluoromethanesulfonate; In acetonitrile; at 20 ℃; for 4h; Inert atmosphere;

Reference yield:

: 3236-71-3
9,9-bis(4-hydroxyphenyl)fluorene

: 1403963-55-2
(S)-1-chloro-3-(4-(9-(4-((R)-2-hydroxy-3-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)propoxy)phenyl)-9H-fluoren-9-yl)phenoxy)propan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C / Inert atmosphere

1.2: 94 h / 20 °C

2.1: cerium(III) chloride heptahydrate / acetonitrile / 3.5 h / Reflux; Inert atmosphere

3.1: bismuth(lll) trifluoromethanesulfonate / acetonitrile / 4 h / 20 °C / Inert atmosphere

With cerium(III) chloride heptahydrate; sodium hydride; bismuth(lll) trifluoromethanesulfonate; In N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 1403963-69-8
(2R,2'R)-2,2'-(4,4'-(9H-fluorene-9,9-diyl)bis(4,1-phenylene))bis(oxy)bis(methylene)dioxirane

: 1403963-55-2
(S)-1-chloro-3-(4-(9-(4-((R)-2-hydroxy-3-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)propoxy)phenyl)-9H-fluoren-9-yl)phenoxy)propan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: cerium(III) chloride heptahydrate / acetonitrile / 3.5 h / Reflux; Inert atmosphere

2: bismuth(lll) trifluoromethanesulfonate / acetonitrile / 4 h / 20 °C / Inert atmosphere

With cerium(III) chloride heptahydrate; bismuth(lll) trifluoromethanesulfonate; In acetonitrile;