(R)-2-<(benzyloxycarbonyl)amino>-2-<(4-methylphenyl)sulfenyl>-3,3,3-trifluoropropanal

Base Information

Chemical Name:(R)-2-<(benzyloxycarbonyl)amino>-2-<(4-methylphenyl)sulfenyl>-3,3,3-trifluoropropanal
CAS No.:176756-69-7
Molecular Formula:C₁₈H₁₆F₃NO₃S
Molecular Weight:383.391
Hs Code.:

Synonyms:(R)-2-<(benzyloxycarbonyl)amino>-2-<(4-methylphenyl)sulfenyl>-3,3,3-trifluoropropanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2-<(benzyloxycarbonyl)amino>-2-<(4-methylphenyl)sulfenyl>-3,3,3-trifluoropropanal

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Technology Process of (R)-2-<(benzyloxycarbonyl)amino>-2-<(4-methylphenyl)sulfenyl>-3,3,3-trifluoropropanal

There total 5 articles about (R)-2-<(benzyloxycarbonyl)amino>-2-<(4-methylphenyl)sulfenyl>-3,3,3-trifluoropropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 169137-91-1
[(Z)-2-((R)-Toluene-4-sulfinyl)-1-trifluoromethyl-vinyl]-carbamic acid benzyl ester

: 176756-69-7
(R)-2-<(benzyloxycarbonyl)amino>-2-<(4-methylphenyl)sulfenyl>-3,3,3-trifluoropropanal

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0.02 h / 0 °C

2: SiO₂, H₂O / 0.17 h / 0 °C

With water; silica gel; In tetrahydrofuran;
DOI:10.1080/10426509708545545

Reference yield:

: [(Z)-2-((S)-Toluene-4-sulfinyl)-1-trifluoromethyl-vinyl]-carbamic acid benzyl ester

: 176756-69-7
(R)-2-<(benzyloxycarbonyl)amino>-2-<(4-methylphenyl)sulfenyl>-3,3,3-trifluoropropanal

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0.02 h / 0 °C

2: SiO₂, H₂O / 0.17 h / 0 °C

With water; silica gel; In tetrahydrofuran;
DOI:10.1080/10426509708545545

Reference yield:

: 197704-06-6
Trifluoro-acetic acid (R)-2-[(E)-benzyloxycarbonylimino]-3,3,3-trifluoro-1-p-tolylsulfanyl-propyl ester

: 176756-69-7
(R)-2-<(benzyloxycarbonyl)amino>-2-<(4-methylphenyl)sulfenyl>-3,3,3-trifluoropropanal

: (S)-2-<(benzyloxycarbonyl)amino>-2-<(4-methylphenyl)sulfenyl>-3,3,3-trifluoropropanal

Guidance literature:: With water; silica gel; at 30 ℃; for 0.0166667h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0957-4166(97)00338-8