Technology Process of N-(2,3-dihydro-1H-inden-5-yl)-N--L-alanyl>glycine t-butyl ester
There total 12 articles about N-(2,3-dihydro-1H-inden-5-yl)-N--L-alanyl>glycine t-butyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
zinc;
In
acetic acid;
for 2.5h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / propan-2-ol
2: dicyclohexylcarbodiimide / CH2Cl2 / Ambient temperature
3: 67 percent / ammonium formate / 10 percent Pd on C / methanol / 0.25 h
4: 1.) 4 A molecular sieves; 2.) sodium cyanoborohydride / 1.) ethanol, 1 h, room temp.; 2.) ethanol, 2.5 h
With
4 A molecular sieve; ammonium formate; sodium cyanoborohydride; triethylamine; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
methanol; dichloromethane; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / propan-2-ol
2: dicyclohexylcarbodiimide / CH2Cl2 / Ambient temperature
3: 67 percent / ammonium formate / 10 percent Pd on C / methanol / 0.25 h
4: 1.) 4 A molecular sieves; 2.) sodium cyanoborohydride / 1.) ethanol, 1 h, room temp.; 2.) ethanol, 2.5 h
With
4 A molecular sieve; ammonium formate; sodium cyanoborohydride; triethylamine; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
methanol; dichloromethane; isopropyl alcohol;
