N-(2,3-dihydro-1H-inden-5-yl)-N--L-alanyl>glycine t-butyl ester

Base Information

Chemical Name:N-(2,3-dihydro-1H-inden-5-yl)-N--L-alanyl>glycine t-butyl ester
CAS No.:84827-75-8
Molecular Formula:C₃₀H₄₀N₂O₅
Molecular Weight:508.658
Hs Code.:

N-(2,3-dihydro-1H-inden-5-yl)-N-<N-<(1S)-1-(ethoxycarbonyl)-3-phenylpropyl>-L-alanyl>glycine t-butyl ester

Synonyms:N-(2,3-dihydro-1H-inden-5-yl)-N--L-alanyl>glycine t-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,3-dihydro-1H-inden-5-yl)-N--L-alanyl>glycine t-butyl ester

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Technology Process of N-(2,3-dihydro-1H-inden-5-yl)-N--L-alanyl>glycine t-butyl ester

There total 12 articles about N-(2,3-dihydro-1H-inden-5-yl)-N--L-alanyl>glycine t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 101843-77-0
N-(2,3-dihydro-1H-inden-5-yl)-N--N-(2,2,2-trichloroethoxycarbonyl)-L-alanyl>-glycine t-butyl ester

: 84827-75-8
N-(2,3-dihydro-1H-inden-5-yl)-N--L-alanyl>glycine t-butyl ester

Guidance literature:: With zinc; In acetic acid; for 2.5h; Ambient temperature;

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 84827-75-8
N-(2,3-dihydro-1H-inden-5-yl)-N--L-alanyl>glycine t-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / propan-2-ol

2: dicyclohexylcarbodiimide / CH₂Cl₂ / Ambient temperature

3: 67 percent / ammonium formate / 10 percent Pd on C / methanol / 0.25 h

4: 1.) 4 A molecular sieves; 2.) sodium cyanoborohydride / 1.) ethanol, 1 h, room temp.; 2.) ethanol, 2.5 h

With 4 A molecular sieve; ammonium formate; sodium cyanoborohydride; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane; isopropyl alcohol;

Reference yield:

: 24425-40-9
indan-5-amine

: 84827-75-8
N-(2,3-dihydro-1H-inden-5-yl)-N--L-alanyl>glycine t-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / propan-2-ol

2: dicyclohexylcarbodiimide / CH₂Cl₂ / Ambient temperature

3: 67 percent / ammonium formate / 10 percent Pd on C / methanol / 0.25 h

4: 1.) 4 A molecular sieves; 2.) sodium cyanoborohydride / 1.) ethanol, 1 h, room temp.; 2.) ethanol, 2.5 h

With 4 A molecular sieve; ammonium formate; sodium cyanoborohydride; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane; isopropyl alcohol;