(3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanone

Base Information

• Chemical Name: (3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanone
• CAS No.: 1638138-06-3
• Molecular Formula: C₁₇H₂₂O₅
• Molecular Weight: 306.359

Synonyms:(3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanone

Chemical Property of (3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanone

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Technology Process of (3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanone

There total 1 articles about (3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanol (1638138-05-2) → (3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanone (1638138-06-3)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; Molecular sieve; Inert atmosphere;

DOI:10.1007/s12039-016-1106-0

Reference yield: 80.0%

(3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanone (1638138-06-3) → (R)-(3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanol (1638138-07-4)

Guidance literature:

(3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanone; With lithium aluminium tetrahydride; In tetrahydrofuran; at -78 ℃; for 0.5h;

With methanol; rochelle salt; In tetrahydrofuran; diethyl ether; at 0 ℃;

DOI:10.1007/s12039-014-0616-x

Reference yield: 80.0%

(3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanone (1638138-06-3) → C17H24O5

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

DOI:10.1007/s12039-016-1106-0

upstream raw materials:

(3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanol

Downstream raw materials:

(2R,3R)-3-(4-methoxybenzyloxy)-3-(3,4-dimethoxyphenyl)propane-1,2-diol

(2R,3R)-3-(4-methoxybenzyloxy)-2-hydroxy-3-(3,4-dimethoxyphenyl)propyl 4-methylbenzenesulphonate

(1R,2R)-1-(4-methoxybenzyloxy)-1-(3,4-dimethoxyphenyl)propan-2-ol

(R)-(3,4-dimethoxyphenyl)((R)-2,2-cyclohexylidene-1,3-dioxolan-4-yl)methanol

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