methyl 3-[(2-chloro-4-{[3-(2,6-dichlorophenyl)-5-isopropyl-4-isoxazolyl]methoxy}anilino)carbonyl]benzoate

Base Information

Chemical Name:methyl 3-[(2-chloro-4-{[3-(2,6-dichlorophenyl)-5-isopropyl-4-isoxazolyl]methoxy}anilino)carbonyl]benzoate
CAS No.:700835-01-4
Molecular Formula:C₂₈H₂₃Cl₃N₂O₅
Molecular Weight:573.86
Hs Code.:

Synonyms:methyl 3-[(2-chloro-4-{[3-(2,6-dichlorophenyl)-5-isopropyl-4-isoxazolyl]methoxy}anilino)carbonyl]benzoate

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Chemical Property of methyl 3-[(2-chloro-4-{[3-(2,6-dichlorophenyl)-5-isopropyl-4-isoxazolyl]methoxy}anilino)carbonyl]benzoate

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Technology Process of methyl 3-[(2-chloro-4-{[3-(2,6-dichlorophenyl)-5-isopropyl-4-isoxazolyl]methoxy}anilino)carbonyl]benzoate

There total 5 articles about methyl 3-[(2-chloro-4-{[3-(2,6-dichlorophenyl)-5-isopropyl-4-isoxazolyl]methoxy}anilino)carbonyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 898253-47-9
4-(bromomethyl)-3-(2,6-dichlorophenyl)-5-isopropyl-isoxazole

: 1383551-51-6
C₁₅H₁₂ClNO₄

: 700835-01-4
methyl 3-[(2-chloro-4-{[3-(2,6-dichlorophenyl)-5-isopropyl-4-isoxazolyl]methoxy}anilino)carbonyl]benzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmcl.2012.04.099

Reference yield:

: 403478-26-2
4-(tert-butyl-dimethyl-silanyloxy)-2-chloro-phenylamine

: 700835-01-4
methyl 3-[(2-chloro-4-{[3-(2,6-dichlorophenyl)-5-isopropyl-4-isoxazolyl]methoxy}anilino)carbonyl]benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: methanesulfonyl chloride; triethylamine / tetrahydrofuran / 0 - 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With tetrabutyl ammonium fluoride; potassium carbonate; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.04.099

Reference yield:

: 1383551-50-5
C₂₁H₂₆ClNO₄Si

: 700835-01-4
methyl 3-[(2-chloro-4-{[3-(2,6-dichlorophenyl)-5-isopropyl-4-isoxazolyl]methoxy}anilino)carbonyl]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.04.099