(2-Oxo-benzothiazol-3-yl)-thioacetic acid S-(2,4,5-trichloro-phenyl) ester

Base Information

Chemical Name:(2-Oxo-benzothiazol-3-yl)-thioacetic acid S-(2,4,5-trichloro-phenyl) ester
CAS No.:72650-13-6
Molecular Formula:C₁₅H₈Cl₃NO₂S₂
Molecular Weight:404.725
Hs Code.:

Synonyms:(2-Oxo-benzothiazol-3-yl)-thioacetic acid S-(2,4,5-trichloro-phenyl) ester

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Chemical Property of (2-Oxo-benzothiazol-3-yl)-thioacetic acid S-(2,4,5-trichloro-phenyl) ester

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Technology Process of (2-Oxo-benzothiazol-3-yl)-thioacetic acid S-(2,4,5-trichloro-phenyl) ester

There total 3 articles about (2-Oxo-benzothiazol-3-yl)-thioacetic acid S-(2,4,5-trichloro-phenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 3773-14-6
2,4,5-trichlorothiophenol

: 881-10-7
2-oxo-3-benzothiazolineacetyl chloride

: 72650-13-6
(2-Oxo-benzothiazol-3-yl)-thioacetic acid S-(2,4,5-trichloro-phenyl) ester

Guidance literature:: With potassium hydroxide; In acetone; at 25 - 30 ℃; for 24h;

Reference yield:

: 934-34-9
2(3H)-Benzothiazolone

: 72650-13-6
(2-Oxo-benzothiazol-3-yl)-thioacetic acid S-(2,4,5-trichloro-phenyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / 25percent aq. NaOH, K₂CO₃ / 1.)90-100 deg C, 6 h 2.)25-30 deg C, 18 h

2: 72 percent / SOCl₂ / benzene / 3 h / Heating

3: 86 percent / 85percent KOH / acetone / 24 h / 25 - 30 °C

With potassium hydroxide; sodium hydroxide; thionyl chloride; potassium carbonate; In acetone; benzene;

Reference yield:

: 945-03-9
(2-oxo-1,3-benzothiazol-3(2H)-yl)acetic acid

: 72650-13-6
(2-Oxo-benzothiazol-3-yl)-thioacetic acid S-(2,4,5-trichloro-phenyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / SOCl₂ / benzene / 3 h / Heating

2: 86 percent / 85percent KOH / acetone / 24 h / 25 - 30 °C

With potassium hydroxide; thionyl chloride; In acetone; benzene;