S-methyl-S-(4-methoxyphenyl)sulfiliminium mesitylenesulfonate

Base Information

Chemical Name:S-methyl-S-(4-methoxyphenyl)sulfiliminium mesitylenesulfonate
CAS No.:108297-57-0
Molecular Formula:C₈H₁₂NOS*C₉H₁₁O₃S
Molecular Weight:369.506
Hs Code.:

Synonyms:S-methyl-S-(4-methoxyphenyl)sulfiliminium mesitylenesulfonate

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Chemical Property of S-methyl-S-(4-methoxyphenyl)sulfiliminium mesitylenesulfonate

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Technology Process of S-methyl-S-(4-methoxyphenyl)sulfiliminium mesitylenesulfonate

There total 3 articles about S-methyl-S-(4-methoxyphenyl)sulfiliminium mesitylenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1879-16-9
1-methoxy-4-methylsulfanyl-benzene

: 36016-40-7
mesitylenesulfonylhydroxylamine

: 108297-57-0
S-methyl-S-(4-methoxyphenyl)sulfiliminium mesitylenesulfonate

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1002/anie.201201296

Reference yield: 45.0%

: 1879-16-9
1-methoxy-4-methylsulfanyl-benzene

: O-(mesitylenesulfonyl)hydroxylamine

: 108297-57-0
C₉H₁₁O₃S^(1-)*C₈H₁₂NOS⁽¹⁺⁾

Guidance literature:: In dichloromethane; at 4 ℃; for 0.75h;
DOI:10.1021/jo00389a012

Reference yield:

: ethyl O-(mesitylenesulfonyl)acetohydroxamate

: 108297-57-0
S-methyl-S-(4-methoxyphenyl)sulfiliminium mesitylenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: perchloric acid / 1,4-dioxane / 0.17 h / 0 °C

2: dichloromethane / 1 h / 0 - 20 °C

With perchloric acid; In 1,4-dioxane; dichloromethane;
DOI:10.1002/anie.201201296