C₁₆H₂₀O₆

Base Information

Chemical Name:C₁₆H₂₀O₆
CAS No.:1313375-30-2
Molecular Formula:C₁₆H₂₀O₆
Molecular Weight:308.331
Hs Code.:

C<sub>16</sub>H<sub>20</sub>O<sub>6</sub>

Synonyms:C₁₆H₂₀O₆

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Chemical Property of C₁₆H₂₀O₆

Chemical Property:

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Technology Process of C₁₆H₂₀O₆

There total 11 articles about C₁₆H₂₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1313375-24-4
C₁₇H₂₂O₆

: 1313375-30-2
C₁₆H₂₀O₆

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/chem.201003402

Reference yield:

: C₃₀H₃₄O₈

: 1313375-30-2
C₁₆H₂₀O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2.1: 1H-imidazole; sodium hydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

3.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

4.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 24 h / Reflux; Inert atmosphere

5.1: hydrogenchloride / ethanol; water / 3 h / Reflux; Inert atmosphere

6.1: pyridine / ethanol / 24 h / 20 °C / Inert atmosphere

7.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 3 h / 45 °C / Inert atmosphere

8.1: tetrabutylammomium bromide; palladium diacetate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 8 h / 85 °C / Inert atmosphere

9.1: sodium methylate / methanol / 20 °C

10.1: water; lithium hydroxide / tetrahydrofuran; methanol; water / 3 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogenchloride; 2,2'-azobis(isobutyronitrile); tetrabutylammomium bromide; water; tri-n-butyl-tin hydride; sodium methylate; palladium diacetate; sodium hydride; sodium hydrogencarbonate; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 8.1: Heck coupling / 9.1: Zemplen reaction;
DOI:10.1002/chem.201003402

Reference yield:

: 1313375-81-3
C₃₅H₄₂O₈S₂

: 1313375-30-2
C₁₆H₂₀O₆

Guidance literature:: Multi-step reaction with 7 steps

1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 24 h / Reflux; Inert atmosphere

2: hydrogenchloride / ethanol; water / 3 h / Reflux; Inert atmosphere

3: pyridine / ethanol / 24 h / 20 °C / Inert atmosphere

4: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 3 h / 45 °C / Inert atmosphere

5: tetrabutylammomium bromide; palladium diacetate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 8 h / 85 °C / Inert atmosphere

6: sodium methylate / methanol / 20 °C

7: water; lithium hydroxide / tetrahydrofuran; methanol; water / 3 h / 20 °C / Inert atmosphere

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; hydrogenchloride; 2,2'-azobis(isobutyronitrile); tetrabutylammomium bromide; water; tri-n-butyl-tin hydride; sodium methylate; palladium diacetate; sodium hydrogencarbonate; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 5: Heck coupling / 6: Zemplen reaction;
DOI:10.1002/chem.201003402