{[4-(tert-butyldimethylsiloxymethyl)-phenyl]-methyl} 2,3,4,6-tetra-O-allyl-β-D-gluco-hexopyranoside

Base Information

Chemical Name:{[4-(tert-butyldimethylsiloxymethyl)-phenyl]-methyl} 2,3,4,6-tetra-O-allyl-β-D-gluco-hexopyranoside
CAS No.:252060-84-7
Molecular Formula:C₃₂H₅₀O₇Si
Molecular Weight:574.83
Hs Code.:

Synonyms:{[4-(tert-butyldimethylsiloxymethyl)-phenyl]-methyl} 2,3,4,6-tetra-O-allyl-β-D-gluco-hexopyranoside

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Chemical Property of {[4-(tert-butyldimethylsiloxymethyl)-phenyl]-methyl} 2,3,4,6-tetra-O-allyl-β-D-gluco-hexopyranoside

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Technology Process of {[4-(tert-butyldimethylsiloxymethyl)-phenyl]-methyl} 2,3,4,6-tetra-O-allyl-β-D-gluco-hexopyranoside

There total 5 articles about {[4-(tert-butyldimethylsiloxymethyl)-phenyl]-methyl} 2,3,4,6-tetra-O-allyl-β-D-gluco-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 252060-83-6
[(4-hydroxymethylphenyl)-methyl] 2,3,4,6-tetra-O-allyl-β-D-gluco-hexopyranoside

: 69739-34-0
t-butyldimethylsiyl triflate

: 252060-84-7
{[4-(tert-butyldimethylsiloxymethyl)-phenyl]-methyl} 2,3,4,6-tetra-O-allyl-β-D-gluco-hexopyranoside

Guidance literature:: With pyridine; In acetonitrile; at 20 ℃;
DOI:10.1021/ol9910619

Reference yield:

: 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl 2,2,2-trichloroacetimidate

: 252060-84-7
{[4-(tert-butyldimethylsiloxymethyl)-phenyl]-methyl} 2,3,4,6-tetra-O-allyl-β-D-gluco-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / dimethylformamide; kerosene / 20 °C

1.2: lithium aluminum hydride / diethyl ether

2.1: 65 percent / pyridine / acetonitrile / 20 °C

With pyridine; sodium hydride; In N,N-dimethyl-formamide; acetonitrile; kerosene; 2.1: Williamson synthesis;
DOI:10.1021/ol9910619

Reference yield:

: 6908-41-4,58590-49-1
4-(methoxycarbonyl)benzyl alcohol

: 252060-84-7
{[4-(tert-butyldimethylsiloxymethyl)-phenyl]-methyl} 2,3,4,6-tetra-O-allyl-β-D-gluco-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / dimethylformamide; kerosene / 20 °C

1.2: lithium aluminum hydride / diethyl ether

2.1: 65 percent / pyridine / acetonitrile / 20 °C

With pyridine; sodium hydride; In N,N-dimethyl-formamide; acetonitrile; kerosene; 2.1: Williamson synthesis;
DOI:10.1021/ol9910619