4-allyloxy-3-(allyl-phenyl-amino)-6-benzo[1,3]dioxol-5-yl-2-methyl-benzoic acid ethyl ester

Base Information

• Chemical Name: 4-allyloxy-3-(allyl-phenyl-amino)-6-benzo[1,3]dioxol-5-yl-2-methyl-benzoic acid ethyl ester
• CAS No.: 1190367-04-4
• Molecular Formula: C₂₉H₂₉NO₅
• Molecular Weight: 471.553

Synonyms:4-allyloxy-3-(allyl-phenyl-amino)-6-benzo[1,3]dioxol-5-yl-2-methyl-benzoic acid ethyl ester

Chemical Property of 4-allyloxy-3-(allyl-phenyl-amino)-6-benzo[1,3]dioxol-5-yl-2-methyl-benzoic acid ethyl ester

Chemical Property:

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Technology Process of 4-allyloxy-3-(allyl-phenyl-amino)-6-benzo[1,3]dioxol-5-yl-2-methyl-benzoic acid ethyl ester

There total 1 articles about 4-allyloxy-3-(allyl-phenyl-amino)-6-benzo[1,3]dioxol-5-yl-2-methyl-benzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-allyloxy-6-benzo[1,3]dioxol-5-yl-2-methyl-3-phenylamino-benzoic acid ethyl ester (1190366-89-2) + allyl bromide (106-95-6) → 4-allyloxy-3-(allyl-phenyl-amino)-6-benzo[1,3]dioxol-5-yl-2-methyl-benzoic acid ethyl ester (1190367-04-4)

Guidance literature:

4-allyloxy-6-benzo[1,3]dioxol-5-yl-2-methyl-3-phenylamino-benzoic acid ethyl ester; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

allyl bromide; In N,N-dimethyl-formamide; at 0 - 25 ℃;

DOI:10.1039/b910397j

Reference yield: 90.0%

4-allyloxy-3-(allyl-phenyl-amino)-6-benzo[1,3]dioxol-5-yl-2-methyl-benzoic acid ethyl ester (1190367-04-4) → 9-benzo[1,3]dioxol-5-yl-7-methyl-6-phenyl-5,6-dihydro-2H-benzo[b][1,4]oxazocine-8-carboxylic acid ethyl ester (1190367-20-4)

Guidance literature:

With Grubbs catalyst first generation; In dichloromethane; at 25 ℃; Inert atmosphere;

DOI:10.1039/b910397j

upstream raw materials:

4-allyloxy-6-benzo[1,3]dioxol-5-yl-2-methyl-3-phenylamino-benzoic acid ethyl ester

allyl bromide

Downstream raw materials:

9-benzo[1,3]dioxol-5-yl-7-methyl-6-phenyl-5,6-dihydro-2H-benzo[b][1,4]oxazocine-8-carboxylic acid ethyl ester

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