2,2'-dibromo-4,4'-bis(phenylethynyl)-3,3',5,5',6,6'-hexafluorobiphenyl

Base Information

Chemical Name:2,2'-dibromo-4,4'-bis(phenylethynyl)-3,3',5,5',6,6'-hexafluorobiphenyl
CAS No.:1095101-37-3
Molecular Formula:C₂₈H₁₀Br₂F₆
Molecular Weight:620.186
Hs Code.:

Synonyms:2,2'-dibromo-4,4'-bis(phenylethynyl)-3,3',5,5',6,6'-hexafluorobiphenyl

Suppliers and Price of 2,2'-dibromo-4,4'-bis(phenylethynyl)-3,3',5,5',6,6'-hexafluorobiphenyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2'-dibromo-4,4'-bis(phenylethynyl)-3,3',5,5',6,6'-hexafluorobiphenyl

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Technology Process of 2,2'-dibromo-4,4'-bis(phenylethynyl)-3,3',5,5',6,6'-hexafluorobiphenyl

There total 1 articles about 2,2'-dibromo-4,4'-bis(phenylethynyl)-3,3',5,5',6,6'-hexafluorobiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 5576-19-2
2,2'-dibromooctafluorobiphenyl

: 4440-01-1
lithium phenylacetylide

: 1095101-37-3
2,2'-dibromo-4,4'-bis(phenylethynyl)-3,3',5,5',6,6'-hexafluorobiphenyl

Guidance literature:: In tetrahydrofuran; for 16h; Inert atmosphere;
DOI:10.1021/jo802171t

Reference yield: 65.0%

: 1095101-37-3
2,2'-dibromo-4,4'-bis(phenylethynyl)-3,3',5,5',6,6'-hexafluorobiphenyl

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 1095101-38-4
2,7-bis(phenylethynyl)-9,9-dimethyl-hexafluorosilafluorene

Guidance literature:: 2,2'-dibromo-4,4'-bis(phenylethynyl)-3,3',5,5',6,6'-hexafluorobiphenyl; With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane; at -78 ℃; for 2h; Inert atmosphere;

dimethylsilicon dichloride; In tetrahydrofuran; diethyl ether; hexane; at -78 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jo802171t

Reference yield: 56.0%

: 1095101-37-3
2,2'-dibromo-4,4'-bis(phenylethynyl)-3,3',5,5',6,6'-hexafluorobiphenyl

: 80-10-4
diphenylsilyl dichloride

: 1095101-41-9
2,7-bis(phenylethynyl)-9,9-diphenyl-hexafluorosilafluorene

Guidance literature:: 2,2'-dibromo-4,4'-bis(phenylethynyl)-3,3',5,5',6,6'-hexafluorobiphenyl; With n-butyllithium; In tetrahydrofuran; diethyl ether; hexane; at -78 ℃; for 2h; Inert atmosphere;

diphenylsilyl dichloride; In tetrahydrofuran; diethyl ether; hexane; at -78 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jo802171t