N-(4-aminobenzyl)-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-amine

Base Information

• Chemical Name: N-(4-aminobenzyl)-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-amine
• CAS No.: 1022171-51-2
• Molecular Formula: C₂₃H₂₈N₄O
• Molecular Weight: 376.502

Synonyms:N-(4-aminobenzyl)-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-amine

Chemical Property of N-(4-aminobenzyl)-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-amine

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Technology Process of N-(4-aminobenzyl)-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-amine

There total 1 articles about N-(4-aminobenzyl)-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

N-(4-nitrobenzyl)-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-amine (1022171-50-1) → N-(4-aminobenzyl)-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-amine (1022171-51-2)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In ethyl acetate; at 20 ℃; for 4h; under 2250.23 Torr; autoclave;

Reference yield: 80.0%

N-(4-aminobenzyl)-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-amine (1022171-51-2) + Cyclobutanecarbonyl chloride (5006-22-4) → N-[4-({[5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-yl]amino}methyl)phenyl]cyclobutanecarboxamide (1022170-68-8)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield: 75.0%

N-(4-aminobenzyl)-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-amine (1022171-51-2) + allylisocyanate (1476-23-9) → N-propyl-2-en-1-yl-N'-[4-({[5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-yl]amino}methyl)phenyl]urea (1022170-69-9)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 6h;

upstream raw materials:

N-(4-nitrobenzyl)-5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-amine

Downstream raw materials:

N-propyl-2-en-1-yl-N'-[4-({[5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-yl]amino}methyl)phenyl]urea

N-[4-({[5-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,4-oxadiazol-2-yl]amino}methyl)phenyl]cyclobutanecarboxamide

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